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《China Journal of Chinese Materia Medica》 2014-14
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Chemical constituents from roots of Illicium majus

NIU Chang-shan;WANG Ya-dan;QU Jing;YU Shi-shan;LI Yong;LIU Yun-bao;MA Shuang-gang;LV Hai-ning;CHEN Xia;XU Song;State Key Laboratory of Bioactive Substance and Function of Natural Medicines,Institute of Materia Medica,Chinese Academy of Medical Sciences and Peking Union Medical College;  
Ten compounds,including seven sesquiterpenes,two phenols and one phenylpropanoid,were isolated from the roots of Illicium majus by means of silica gel,ODS,Sephadex LH-20,and preparative HPLC. On analysis of MS and NMR spectroscopic data,their structures were established as cycloparviflorolide( 1),cycloparvifloralone( 2),tashironin( 3),tashironin A( 4),anislactone A( 5),anislactone B( 6),pseudomajucin( 7),syringaldehyde( 8),methyl-4-hydroxy-3,5-dimethoxybenzoate( 9),and( E)-3-methoxy-4,5-methylenedioxycinnamic alchol( 10),respectively. Compounds 1-4 and 8-10 were first isolated from this plant. In the in vitro assays,at a concentration of 1. 0 × 10-5mol·L-1,compounds 5 and 6 were active against LPS induced NO production in microglia with a inhibition rate of 75. 31% and 53. 7%,respectively.
【Fund】: 国家自然科学基金项目(21132009)
【CateGory Index】: R284
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