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《Chinese Journal of Health Laboratory Technology》 2009-10
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HPLC for rapid identification of xiaokewan and limited inspection of glibenclamide

WANG Xiao-ling1,LI Ying-hui2,GUO Luo-hong1(1.Institute for Food and Drug Control of Luoyang,Luoyang 471023,China;2.Huanghe College of Science and Technology,Zhengzhou 450000,China)  
Objective:To establish a HPLC method for the rapid identification of Xiaoke wan and glibenclamide limited examination.Methods:HPLC identification of Xiaoke wan used Hypersil BDS C18 column(4.6 mm×150 mm,5 μm),acetonitrile: 0.1% phosphoric acid aqueous solution,non-linear process gradient elution,detection wavelength 235 nm,theoretical plate number is greater than 3000;of glibenclamide to check the use of limited Hypersil ODS C18 column(4.6 mm×200 mm,5 μm),methanol: ammonium dihydrogen phosphate solution elution,detection wavelength 230 nm,theoretical plate number is greater than 6000.Results:Qualitative Xiaoke wan identification of the HPLC to Deoxyschizandrin,puerarin,glibenclamide qualitative indicators as a reference substance,HPLC method able to distinguish the authenticity of Xiaoke wan;Glibenclamide detection limit for 50.2 ng/ml.Conclusion:The method is easy to detect specific,reproducible,and can be used for quality control Xiaoke wan.
【Key Words】: Xiaoke wan HPLC Deoxyschizandrin Puerarin Glibenclamide limited inspection
【CateGory Index】: R286;R927
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【Citations】
Chinese Journal Full-text Database 2 Hits
1 FENG Xin1,2,XIANG Lan1,JIN Chuan-shan2(1.School of Pharmaceutical Sciences,Shandong University,Jinan 250012,China;2.Anhui College of Traditional Chinese Medicine,Hefei 230001,China);Determination of puerarin in xiaoke pill by HPLC[J];Anhui Medical and Pharmaceutical Journal;2008-03
2 CHEN You-hua1,HUANG Xun-rui2(Ningde Institute For Drug Control,Ningde 352100,China);Determination of Pueranin in Xiaokewan by HPLC[J];Strait Pharmaceutical Journal;2007-08
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 HU An-qing (Zhenjiang Institute for Drug Control,Zhenjiang,Jiangsu Province 212003);Determination of puerarin in ganmaozhike granule by HPLC[J];Anhui Medical and Pharmaceutical Journal;2007-11
2 LIU Tong-xiang,AN Wei(Institute of Chinese Minority Traditional Medicine,Central University for Nationalities,Beijing 100081,China);Content Determination of Berberine Hydrochloride in Qianlietong Soft Capsules by High Performance Liquid Chromatography[J];Journal of Anhui Traditional Chinese Medical College;2009-04
3 ;Determination of substances in citicoline sodium glucose injection by ion-paired HPLC[J];Academic Journal of Second Military Medical University;2005-04
4 TU Bo~1,WANG Li~2(1.Department of Chemistry,Guiyang Medical College,Guiyang 550004,China;2.Guiyang Maidike Medical Science and Technology Development Institute,Guiyang 550002,China);Determination of Geniposide in Fushenning Capsule by HPLC[J];Journal of Guiyang Medical College;2006-01
5 Feng Binbin,Zhang Jianmei,Zhu Huifeng,et al TCM College of Xinan University,Chongqing(400716);Quality Standard Study on Danqi Tablets[J];Journal of Zhejiang University of Traditional Chinese Medicine;2010-01
6 HE Jian-hua,QIAN Yong-chang,XU-Yong(JiangYan Hospital of Traditional Chinese Medicine,JiangSu Province,225500,China);Determination of Puerarin in Jingbi Granules by HPLC[J];Strait Pharmaceutical Journal;2005-06
7 LI Dao-ming(Xinyang Institute for Food and Drug control of Henan province,Xinyang 464000,China);Study on the bacterial endotoxins test of Shenmai injection[J];Strait Pharmaceutical Journal;2008-03
8 RUAN Guo-hu1,ZHAO Tie1,JIAN Ling-yan1,XU Ying-hong1,LI Yu-ling1,MENG Fan-hao2(1.Department of Pharmacy,the Affiliated Shengjing Hospital,China Medical University,Shenyang 110004,China;2.School of Pharmacy,China Medical University,Shenyang 110001,China);Determination of Puerarin in Qingre Mistura by HPLC[J];Chemistry & Bioengineering;2007-02
9 CHENG Zhi,LIU Chunyyan;Effect of Essential Oil on Prevention of Pressure Ulcers[J];Journal of Nursing Science;2009-14
10 LIU Jing 1,WANG Yun fang 1,ZHANG Xiao yu 2,GAO Sheng li 2 (1.Department of Chemistry,Xian Yang Teachers College,Xianyang 712000,China; 2.Department of Chemistry,North West University,Xi'an 710069,China);Phase Equilibrium Study on Ternary System of Zn(NO_3)_2-Val-H_2O[J];Natural Science Journal of Hainan University;2002-02
【Secondary Citations】
Chinese Journal Full-text Database 4 Hits
1 XU Jia-gen 1,CHU Li-mei 1,LU Ji-hao 2 (1.The Affiliated Nanjing children's Hospital of Nanjing Medical University,Nanjing 210008; 2.Nanjing Xinye Medicinal Technology Co.Ltd,Nanjing 210014,China);Eetermination of kakonein in ganmaoqingre granules by RP-HPLC[J];Anhui Medical and Pharmaceutical Journal;2005-03
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