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《Chinese Journal of Health Laboratory Technology》 2009-10
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HPLC for rapid identification of xiaokewan and limited inspection of glibenclamide

WANG Xiao-ling1,LI Ying-hui2,GUO Luo-hong1(1.Institute for Food and Drug Control of Luoyang,Luoyang 471023,China;2.Huanghe College of Science and Technology,Zhengzhou 450000,China)  
Objective:To establish a HPLC method for the rapid identification of Xiaoke wan and glibenclamide limited examination.Methods:HPLC identification of Xiaoke wan used Hypersil BDS C18 column(4.6 mm×150 mm,5 μm),acetonitrile: 0.1% phosphoric acid aqueous solution,non-linear process gradient elution,detection wavelength 235 nm,theoretical plate number is greater than 3000;of glibenclamide to check the use of limited Hypersil ODS C18 column(4.6 mm×200 mm,5 μm),methanol: ammonium dihydrogen phosphate solution elution,detection wavelength 230 nm,theoretical plate number is greater than 6000.Results:Qualitative Xiaoke wan identification of the HPLC to Deoxyschizandrin,puerarin,glibenclamide qualitative indicators as a reference substance,HPLC method able to distinguish the authenticity of Xiaoke wan;Glibenclamide detection limit for 50.2 ng/ml.Conclusion:The method is easy to detect specific,reproducible,and can be used for quality control Xiaoke wan.
【CateGory Index】: R286;R927
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