Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chinese Journal of Health Laboratory Technology》 2009-10
Add to Favorite Get Latest Update

HPLC for rapid identification of xiaokewan and limited inspection of glibenclamide

WANG Xiao-ling1,LI Ying-hui2,GUO Luo-hong1(1.Institute for Food and Drug Control of Luoyang,Luoyang 471023,China;2.Huanghe College of Science and Technology,Zhengzhou 450000,China)  
Objective:To establish a HPLC method for the rapid identification of Xiaoke wan and glibenclamide limited examination.Methods:HPLC identification of Xiaoke wan used Hypersil BDS C18 column(4.6 mm×150 mm,5 μm),acetonitrile: 0.1% phosphoric acid aqueous solution,non-linear process gradient elution,detection wavelength 235 nm,theoretical plate number is greater than 3000;of glibenclamide to check the use of limited Hypersil ODS C18 column(4.6 mm×200 mm,5 μm),methanol: ammonium dihydrogen phosphate solution elution,detection wavelength 230 nm,theoretical plate number is greater than 6000.Results:Qualitative Xiaoke wan identification of the HPLC to Deoxyschizandrin,puerarin,glibenclamide qualitative indicators as a reference substance,HPLC method able to distinguish the authenticity of Xiaoke wan;Glibenclamide detection limit for 50.2 ng/ml.Conclusion:The method is easy to detect specific,reproducible,and can be used for quality control Xiaoke wan.
【Key Words】: Xiaoke wan HPLC Deoxyschizandrin Puerarin Glibenclamide limited inspection
【CateGory Index】: R286;R927
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 2 Hits
1 FENG Xin1,2,XIANG Lan1,JIN Chuan-shan2(1.School of Pharmaceutical Sciences,Shandong University,Jinan 250012,China;2.Anhui College of Traditional Chinese Medicine,Hefei 230001,China);Determination of puerarin in xiaoke pill by HPLC[J];Anhui Medical and Pharmaceutical Journal;2008-03
2 CHEN You-hua1,HUANG Xun-rui2(Ningde Institute For Drug Control,Ningde 352100,China);Determination of Pueranin in Xiaokewan by HPLC[J];Strait Pharmaceutical Journal;2007-08
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 DAI Jun et al (Jiangsu Zhongxing Pharmaceutical Co.,Ltd.,Zhengjiang,Jiangsu 212009);Determination of the Glibenclamide in Poria and Rhizoma Dioscoreae Tablets by TLC-Scanning[J];Journal of Anhui Agricultural Sciences;2010-36
2 HU An-qing (Zhenjiang Institute for Drug Control,Zhenjiang,Jiangsu Province 212003);Determination of puerarin in ganmaozhike granule by HPLC[J];Anhui Medical and Pharmaceutical Journal;2007-11
3 LIU Tong-xiang,AN Wei(Institute of Chinese Minority Traditional Medicine,Central University for Nationalities,Beijing 100081,China);Content Determination of Berberine Hydrochloride in Qianlietong Soft Capsules by High Performance Liquid Chromatography[J];Journal of Anhui Traditional Chinese Medical College;2009-04
4 Feng Binbin,Zhang Jianmei,Zhu Huifeng,et al TCM College of Xinan University,Chongqing(400716);Quality Standard Study on Danqi Tablets[J];Journal of Zhejiang University of Traditional Chinese Medicine;2010-01
5 ;Determination of substances in citicoline sodium glucose injection by ion-paired HPLC[J];Academic Journal of Second Military Medical University;2005-04
6 XIAO Yuting,ZHAO Mingfen,PENG Fang,XIAO Peiyun(College of Pharmacy,Dali University,Dali,Yunnan 671000,China);Research of the Quality Control Method of the Xiangguojianxiao Tablets Ⅰ:Indentification and Determination of the Major Components of Valeriana Jatamansi Jones[J];Journal of Dali University;2010-08
7 SHEN Liwen,LI Kuaqiao,SUN Yanfen,XIAO Peiyun(College of Pharmacy,Dali University,Dali,Yunnan 671000,China);The Quality Control Method of Xiangguojianxiao Tablets Ⅱ: Identifying and Determining the Main Components of Costustroot in Xiangguojianxiao Tablets[J];Journal of Dali University;2010-12
8 ZHAO Mingfen,SUN Yanfen,XIAO Yuting,LIU Jiabao,Xiao Peiyun(College of Pharmacy and Chemistry,Dali University,Dali,Yunnan 671000,China);Content Determination of Gentiopicroside in Boyunding[J];Journal of Dali University;2011-06
9 Hu Jing1,Yi Fanli2,Liu Songqing1(1Department of Pharmacy,Southwest Hospital,Third Military Medical University,Chongqing,400038;2 Tianjin University of Traditional Chinese Medicine,Tianjin,300193,China);Identification of five active ingredients and content determination of piperine in Shiwuwei Heyaowan pills by TLC and HPLC[J];Journal of Third Military Medical University;2011-06
10 FAN Hui1,2,GU Quan-lin1,HE Zi-wei2,HUANG Rui2,BEI Wei-jian1(1.Institute of Chinese Medicinal Sciences;2.School of Pharmacy,Guangdong Pharmaceutical University,Guangzhou 510006,China);Determination of stilbene glucoside in Wushen Xingnao drop pill by HPLC[J];Journal of Guangdong Pharmaceutical University;2011-06
China Proceedings of conference Full-text Database 1 Hits
1 BAO Xiao-hua1,Bagenna1,BAI Ming-gang1 (1.College of Mongolian Medicine and Pharmacy,Inner University for Nationalities,Tongliao 028000,China);Origin and Advance for MONGOLIAN Medicine Xieriga Decoction of Four Drugs[A];[C];2010
【Secondary Citations】
Chinese Journal Full-text Database 4 Hits
1 XU Jia-gen 1,CHU Li-mei 1,LU Ji-hao 2 (1.The Affiliated Nanjing children's Hospital of Nanjing Medical University,Nanjing 210008; 2.Nanjing Xinye Medicinal Technology Co.Ltd,Nanjing 210014,China);Eetermination of kakonein in ganmaoqingre granules by RP-HPLC[J];Anhui Medical and Pharmaceutical Journal;2005-03
2 HU An-qing (Zhenjiang Institute for Drug Control,Zhenjiang,Jiangsu Province 212003);Determination of puerarin in ganmaozhike granule by HPLC[J];Anhui Medical and Pharmaceutical Journal;2007-11
3 LIU Sheng-jie, WANG Li-na, DONG Sheng-hui( Department of Pharmacy, The General Hospital of PLA,Beijing 100853, China);Determination of puerarin in puerariae radix dripping pills by HPLC[J];Journal of Pharmaceutical Practice;2006-03
4 Tan Shengjian Qiu Xia Li Guanghui Zhao Bingcheng Liang Yuqin(Institute for Durg Control of Commission of Science,Technology and Industry for National Defence,Beijing 100101);Determination of Puerarin in Gegen Qinlian Tablets by RP-HPLC[J];China Journal of Chinese Materia Medica;1996-12
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved