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《Chinese Journal of Health Laboratory Technology》 2011-02
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Simultaneous determination of tin and bismuth in medicinal and edible Chinese medicinal materials by hydride generation-atomic fluorescence spectrometry

JIN Bo,MA Chen(Institute of Materia Medica,Chinese Academy of Medical Sciences and Peking Union Medical College,Beijing 100050,China)  
Objective:A method for simultaneous determination of tin and bismuth in medicinal and edible chinese medicinal materials by hydride generation-atomic fluorescence spectrometry(HG-AFS) was proposed.Methods: The samples were digested by mixed acid of HNO3,HClO4 and H2SO4 in colorimetric tubes and the hydride generation occurred in tartaric acid medium with chosen conditions of carrier,NaBH4 concentration and masking agent.Results: The detection limit of tin and bismuth is 0.18 ng/ml and 0.06 ng/ml.The recovery and precision of tin is 99.0%~105.4% and 0.64%,of Bismuth is 95.0%~97.5% and 0.94%.Conclusion: This method is proved to be repeatable,simple and rapid,and which is suitable for the analysis of tin and bismuth in medicinal materials.
【Fund】: 科技部新药创制重大专项(2009ZX09301-003-7-1):创新药物研究开发技术平台建设 科技部创新方法工作专项(2009IM031600):保健食品中有害物质快速分析检测体系建立
【CateGory Index】: R284.1;O657.31
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