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《Chinese Journal of Rare Metals》 2009-01
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Zirconium Powder Prepared by Fused Salt Electrolysis

Wu Yanke,Chen Song,Xu Zhigao,Wang Lijun*(Division of Mineral Resources,Metallurgy & Materials,General Research Institute for Non-ferrous Metals,Beijing 100088,China)  
The change of the morphology and the size of zirconium powder were studied in the process of preparing zirconium powder by fused salt electrolysis.The melting point and it is change of the electrolyte in electrolysis were defined.The zirconium powder were researched respectively by differential scanning calorimetry analysis,size analysis and chemistry analysis,the morphology of zirconium powder was gotten in the first 2 h electrolysis is irregular and the size is 20~60 μm,in the later 2 h is dendrite and the size is about 100 μm.The effect on morphology,size and the purity of zirconium powder were studied in different electrolysis conditions,and more than 99% purity of zirconium powder was gotten.
【CateGory Index】: TB383.3
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