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《Journal of Chinese Medicinal Materials》 2013-09
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Study on Quality Standard of Chimonanthus nitens Leaf

ZHOU Bin;LI Meng-jie;WANG Ping;CHENG Dan;LI Jie;CUI Xiao-di;School of Pharmacy,Jiangxi Science and Technology Normal University;  
Objective: To set up the quality standard of Chimonanthus nitens leaf. Methods: Five compounds were identified by double-development thin layer chromatography,the plate was colorized with 1% vanillin-H2SO4solution and warmed up in 110 ℃; The content of four compounds was determined by HPLC,the chromatography separation was performed on the Elite hypersil ODS2( 250 mm× 4. 6 mm,5 μm) column with gradient elution. The mixture of acetonitrile and water as the mobile phase at a flow rate of 1. 0 mL / min was used,the detection wavelength was 344 nm and the column temperature was set at 40 ℃. Results: The TLC identification was highly specific and spots were clear. In HPLC method,the calibration curve was linear in the range of 5. 665 ~ 56. 65 μg / mL for scopoletin( r = 0. 9999),the average recovery was 97. 06% and RSD was 1. 27%; The calibration curve was linear in the range of 2. 4312~ 24. 312 μg / mL for isofraxidin( r = 0. 9999),the average recovery was 102. 86% and RSD% was 0. 93%; The calibration curve presented a linear range from 2. 444 ~ 24. 44 μg / mL for scoparone( r = 0. 9999),the average recovery was 102. 18% and RSD was1. 81%. The standard curve presented a linear range from 9. 012 ~ 90. 12 μg / mL for rutin( r = 0. 9992),the average recovery was104. 44% and RSD was 4. 2%. Conclusion: These methods are reproducible,sensitive and simple and can be used to control the quality of Chimonanthus nitens leaf.
【Fund】: 江西省教育厅资助项目(12750);; 江西科技师范大学校级科研项目(Ky2012zy17)
【CateGory Index】: R286.0
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