Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Henan University of Technology(Natural Science Edition)》 2008-01
Add to Favorite Get Latest Update

STUDY ON SYNTHESIS OF I NSECTICIDE NOVALURON

ZHOU Yan-feng,GAO Zhong-liang,QIU Ji-ping,WEN Zi-qiang (School of Chemical Engineering and Technology,Hebei University of Technology, Tianjin 300130,China)  
2-chloro-4-aminophenol was synthesized from 2-chloro-4-nitrophenol by reduction reaction,afterwards the addition reaction with perfluoro-vinyl-perfluoro-methyl ether was conducted to synthesize 3-chloro-4-[1,1,2-trifluoro2-(trifluoromethoxy)-ethoxy]aniline.An acylation reaction based on 2,6-difluorobenzamide and oxalyl dichloride was carried out to produce 2,6-difluorobenzoyl isocyanate,afterwards the addition reaction with 3-chloro-4-[1,1,2-trifluoro2-(trifluoromethoxy)-ethoxy]aniline was conducted to synthesize insecticide Novaluron. The overall yield was 68.9%.
【CateGory Index】: TQ453.2
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 6 Hits
1 FENG Gui-rong1,ZHANG Xiang-ping1,ZHANG Hui-ru2 , ZHANG Jian-wei 1 (1. Department of Chemistry, Tangshan Normal College, Tangshan 063000,China; 2.No. 26 Middle School of Tangshan, Tangshan 063000,China);Synthesis of Diarylurea Derivatives[J];Hebei Chemical Engineering and Industry;2005-05
2 WEI Hong tao, TAN Xiao song, TIAN De mei, ZHU Zheng fang (Institute of Organic Synthesis, Central China Normal University, Wuhan 430079)$$$$;Studies on the Preparation of Benzoyl Isocyanates[J];HUNAN CHEMICAL INDUSTRY;2000-05
3 LIU Chang chun (Jiangsu food College, Huaian 223001, China);Synthesis of Insecticide Triflubenzuron[J];Fine Chemical Intermediates;2001-06
4 Mao Deshou et al. (Department of Applied Chemistry, Yunnan University, Kunming 650091 );Recent Development of Benzoyl Urea Chitin Synthesis Inhibitors[J];Pesticides;2001-04
5 JIA Jian-Hong, SHENG Wei-Jian, GAO Jian-Rong(College of Chemical Engineering and Materials, Zhejiang University of Technology, Hangzhou 310032, China);Synthesis of the Benzoylurea Insecticide Teflubenzuron[J];Pesticides;2005-06
6 Zhu Zhixiang et al (East China University of Science and Technology,Shanghai 200237);Study on the Synthesis and Crystal Structure of Triflubenzuron[J];PESTICIDES;1998-12
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 CHEN Wei-Guo1 DONG Rui-Hua1 SUN Hai-Yan1 DAI Jian-Zhong1 ZHU Hao-Long1 WU Fu-An2 (1Haining Sericulture Technology Extension Station of Zhejiang Province,Haining Zhejiang 314400,China;2The Sericultural Research Institute,Chinese Academy of Agricultural Sciences,Zhenjiang Jiangsu 212018,China);An Investigation on Toxicity of the Agricultural Pesticide Chlorantraniliprole to the Silkworm,Bombyx mori[J];Science of Sericulture;2010-01
2 YANG Xin-ling, LING Yun, WANG Dao-quan, CHEN Fu-heng (Department of Applied Chemistry, China Agriculture University, Key Laboratory of Pesticide Chemistry and Application Technology, Beijing 100094, China);The Synthesis and Biological Activity of N-phenyl-N'-(5-phenyl-2-furoyl) Ureas[J];Chinese Journal of Synthetic Chemistry;2002-06
3 JIANG Lin,WANG Li-zeng,WANG Li-yin,XIE Xian-ye(College of Chemistry and Material Science,Shandong Agricultural University,Tai'an 271018,China);Synthesis of N-substituted-phenyl-N′-(1-methyl-3-ethyl-4-chloro-5-pyrazole-formyl)(thio)urea and Their Acaricidal Activity[J];Chinese Journal of Synthetic Chemistry;2007-05
4 Lu Yang~(1,2) Li Chunren~3 Tao Jingzhao~1 Ma Li~4 Xu Guhua~2(1.Chemistry Department of Zhengzhou University,Henan Zhengzhou 450001;2.Office of Organic Chemistry,Xinyang Agriculture College,Henan Xingyang 464000;3.Chemical Engineering Department of Xinyang Vocational andTeehnical College,Henan Xinyang 464000;4.Henan Province Fubang Pesticides Chemical EngineeringCompany Manager,Henan Xinyang 464000);Preparation of Isoproduron as Herbicides Using Non-isocyanate Method[J];Chemical Industry Times;2006-06
5 LIU Chang chun (Jiangsu food College, Huaian 223001, China);Synthesis of Insecticide Triflubenzuron[J];Fine Chemical Intermediates;2001-06
6 SONG Chang-you1,XU Xiu-jun2 (1.Department of Environmental and Chemical Engineering,Tangshan College,Tangshan 063000,China; (2.Department of Teaching and Research Section of Chemistry,Tangshan Vocation & Technical College,Tangshan 063000,China);Synthesis of triflumuron[J];Chemical Engineer;2005-04
7 LI Xiang-gao,ZHU Dong-gang,HE Li-li,WANG Shi-rong(School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China);Synthesis of Phenylurea Derivatives[J];Chemical Industry and Engineering;2009-01
8 Li Ying Cui Zining Hu Jun Ling Yun Yang Xinling~(**)(Key Laboratory of Pesticide Chemistry and Application Technology,MOA,Department of Applied Chemistry,College of Science,China Agricultural University,Beijing 100094,China);Studies on Chitin Synthase Inhibitors[J];Progress in Chemistry;2007-04
9 Wang Tao *1,2 , Ye Wenfeng 2,He Hongwu 1 (1. Institute of Organic Synthesis, Central China Normal University, Wuhan 430079; 2. Department of Chemistry, Yichun College, Yichun 336000);Preparation of isocyanates, isothiocyanates and isoselenocyanates in the laboratory[J];Chemical Reagents;2002-04
10 Li Xinghai, Ling Yun, Yang Xinling * (Department of Applied Chemistry,China Agricultural University,Beijing 100094,China);Synthesis of Novel Benzoyl Ureas Containing Thiadiazole and their Insecticidal Activity[J];Chemistry;2003-05
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 CHENG Shui ming 1,SONG Jia yong 1,YAN Yao li 1, XIA Guo jun 1,ZHANG Gui lan 2 (1 National Engineering Research Center for Wheat,Henan Zhengzhou 450002,China; 2 Soil and Fertilizer Service Station of Henan,Zhengzhou 450002,China);A Study on the Activity of Four New N-Nitroanilinelic Compounds to Plant Pathogenic Fungi[J];Acta Agriculturae Boreall—sinica;2001-02
2 ZHAO Chun1,LI Shuiqing1,XIE Jiugao2 (1.Department of Environmental Engineering,Hubei Agricultural College,Jingzhou,Hubei 434025, China;2.Department of Sciences,Huazhong Agricultural University,Wuhan,Hubei 430070,China);The Synthesis of N-nitrophenyl Urea Derivative[J];Journal of Hubei Agricultural College;2003-05
3 Liu,Chang Ling Lei,Xin Liu,Wu Cheng Zhao,Ri Jin (Shenyang Research Institute of Chemical Industry,Shenyang,110021);Synthesis of Some Novel Pyrazolecarbonylureas and Their Biological Activities[J];CHINESE JOURNAL OF SYNTHETIC CHEMISTRY;1997-04
4 Zhao Xinyun, Zhang Zhengwen, Wang Yangang * (College of Central China Normal University,Wuhan 430079,China);Biological Activities and Synthetic Methods of Acyl Urea Compounds[J];Chemistry;2003-11
5 SUQiu fang (Dept.ofPetrochemicalEngineering ,GuangdongCollegeofPetrochemicalTechnology ,Maoming5 2 5 0 0 0 ,China);Study on synthesis of unsymmetrical aromatic disubstituted ureas[J];JOURNAL OF JILIN INSTITUTE OF CHEMICAL TECHNOLOGY;2000-03
6 WANG WEI-ZHUAN; CHEN WEI-PING; LU SHU-QIN; QI YAO-KUI(Institute of Plant Protection, Cuangdong Academy of Agricultural Sciences, Guangzhou 510640);INSECTICIDAL ACTIVITY OF CHITIN SYNTHESIS INHIBITORSAGAINST DIAMONDBACK MOTH, PLUTELLA XYLOSTELLA[J];ACTA ENTOMOLOGICA SINICA;1994-03
7 PAN Bin 1,FAN Hua 2,FENG Rong-hua 2 (1.Guangdong Chemical Engineering School,Guangzhou 510320,China; 2.Nanchang University,Nanchang 330029,China);Study on a New Technology for Synthesis of TCC[J];Journal of Nanchang University(Engineering & Technology);2002-02
8 CHENG Shui ming 1,XIE Jiu gao 2 (1.National Engineering Research Center for Wheat,Henan Agricaltural University,Zhengzhou 450002,China; 2.Huazhong Agricultural University,Wuhan 430070,China);Studies on biological activity of N-nitro-N-hexhydrogen indole-2,4,6-trichloroabiline[J];Journal of Henan Agricultural University;2001-03
9 Huang Chi; et al.(College of Chemistry, Wuhan University, Wuhan 430072);Research on the Synthesis for 2,6-Difluorobenzamide[J];PESTICIDES;1998-11
10 LiuXinheetal (DeptofChemicalEngineering ,HuaihaiInstituteofTechnology , Lianyungang 2 2 2 0 0 5 );Synthesis of Pyrazosulfuron -ethylbyNon - phos gene Method[J];Pesticides;2000-12
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved