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《JOURNAL OF ANHUI NORMAL UNIVERSITY(NATURAL SCIENCE)》 2000-01
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MICROWAVE SYNTHESIS OF MONODISPERSE POLYSTYRENE MICROSPHERES WITH LARGE SIZE

YOU Li sha,\ ZHANG Wen min (Department of Chemistry, Anhui Normal University, 241000,Wuhu, Anhui, China)  
Polystyrene microspheres with large size were prepared in ethanol medium in the presence of polyvinylpyrrolidone and cetyl alcohol using 4,4' Azo bis(4cyanovaleric) acid or azobisisobutyronitrile as initiator. Monodisperse microspheres with 1~2.5μm in diameter were obtained. The effect of the concentration of the initiator on the particle diameter was discussed. It was found that the rate of polymerization was accelerated and the particle had a narrow distribution of the diameter under microwave radiation.
【Fund】: 国家自然科学基金资助项目
【CateGory Index】: O632
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