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《Journal of Anhui Normal University(Natural Science)》 2004-01
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SYNTHESIS AND STRUCTURE OF 1,1-DIPHENYL-2- (p-TOLYLSULFONYL)ETHENE

XIE Mei-hua,LIU Li(College of Chemistry and Material Sience, Anhui Normal University, Wuhu 241000,China)  
The title compound was synthesized by the carbomagnesiation of phenylmagnesium bromide and 2-phenyl-1-(p-tolylsulfonyl)ethyne. The title compound was characterized by~1H NMR,IR and MS. The single crystal structure was determined by X-ray diffraction analysis. Crystal crystallizes in monoclinic, space group P2(1)/c with unit cell parameters: a=12.8256(6),b=5.8678(7), c=23.871(3)?;α=90°,β=105.360(3)°,γ=90°, V=1732.3(4)?~3,T=293K, Z=4, Dc=1.282g·cm~(-1),μ=0.196mm~(-1), (λ=0.71073?, F(000)704. The final R=0.0427, wR=0.0461,10150 independent were collected, of which 4060 independent reflections with I2σ(I) were used.
【Fund】: 安徽省高校青年教师科研资助计划项目(20038jgl08);; 安徽师范大学博士启动基金资助项目.
【CateGory Index】: O625
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【References】
Chinese Journal Full-text Database 2 Hits
1 JIA Wei-guo (College of Chemistry and Materials Science, Anhui Normal University, Wuhu 241000, China);THE AFFECT OF LIGAND SHAPE TO RARE EARTH METAL Gd~Ⅲ COMPLEXES WITH AMINOCARBOXYLIC ACIDS ON COORDINATION STRUCTURES AND COORDINATION NUMBERS[J];Journal of Anhui Normal University(Natural Science);2004-04
2 XIE Mei-hua,SUN Ying,GU Xiao-xia,ZHAO Xin-yang,ZHANG Wei,XIE Fa-dong(College of Chemistry and Materials Science,Anhui Normal University,Wuhu 241000,China);Synthesis and Crystal Structure of (E)-5-Phenyl-5-(p-Tolyl)-4-(p-Tolylsulfonyl)-1,4-Pentadiene[J];Journal of Anhui Normal University(Natural Science);2008-01
【Co-references】
Chinese Journal Full-text Database 4 Hits
1 WANG Jun *, LIU Zhen-Rong, ZHANG Xiang-Dong, JIA Wei-Guo(Department of Chemistry, Liaoning University, Shenyang 110036, China);Syntheses and Crystal Structures of K_3[Gd~Ⅲ(nta)_2(H_2O)]·6H_2O and (NH_4)·[Gd~Ⅲ(Cydta)(H_2O)_2]·5H_2O[J];Chemical Research In Chinese Universities;2002-11
2 WANG Rui\|Yiao, ZHANG Hua\|Jie, JIN Tian\|Zhu\+* (State Key Laboratory of Rare Earth Materials Chemistry and Applications,\= Peking University, Beijing, 100871) ZHOU Zhong\|Yuan,\ ZHOU Xiang\|Ge (Chengdu Institute of Organic Chemistry, Chinese;Synthesis and Crystal Structure of Gadolinium Mononuclear\= Complex with Triethylenetetraaminehexaacetic Acid[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;1999-02
3 CHEN De-Fu YANG Wei-Chun WANG Rui-Yao JIN Tian-Zhu(Research Center of Rare Earth Chemistry, Peking University, State Key Laboratory of Rare Earth Materials Chemistry and Applications, Beijing, 100871);Synthesis and Crystal Structure of Gadolinium Complex with Triethylenetetraaminehexaacetic Acid[J];Acta Chimica Sinica;1997-07
4 LIN Hong xia, CHEN Qi (School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China);Review of contrast agents used for magnetic resonance imaging[J];Journal of Shenyang Pharmaceutical University;2002-02
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