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《Journal of Anhui Normal University(Natural Science)》 2004-01
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XIE Mei-hua,LIU Li(College of Chemistry and Material Sience, Anhui Normal University, Wuhu 241000,China)  
The title compound was synthesized by the carbomagnesiation of phenylmagnesium bromide and 2-phenyl-1-(p-tolylsulfonyl)ethyne. The title compound was characterized by~1H NMR,IR and MS. The single crystal structure was determined by X-ray diffraction analysis. Crystal crystallizes in monoclinic, space group P2(1)/c with unit cell parameters: a=12.8256(6),b=5.8678(7), c=23.871(3)?;α=90°,β=105.360(3)°,γ=90°, V=1732.3(4)?~3,T=293K, Z=4, Dc=1.282g·cm~(-1),μ=0.196mm~(-1), (λ=0.71073?, F(000)704. The final R=0.0427, wR=0.0461,10150 independent were collected, of which 4060 independent reflections with I2σ(I) were used.
【Fund】: 安徽省高校青年教师科研资助计划项目(20038jgl08);; 安徽师范大学博士启动基金资助项目.
【CateGory Index】: O625
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