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《Glass & Enamel》 1992-01
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Effect of F~- and S~(2-) on the Crystallization Process of CaO-Al_2O_3-SiO_2 System

Zhou Shigui Gu Wenjie Wang Cong Hou Fengzhen (East China Institute of Chemical Technology)Teng Lidong (Shandong Institute of Light Industry)  
In this paper,the effect of F~ and S2-ions on phase separation and crystallization of CaO-Al2O3-SiO2 system glass is studied by means of DTA,IB spectroseopy,XRD,DTEM and EDX.The results show that with the increase of the contents of F-phase separation of the glass intensifies,the microstructure changes and the crystallization temperature(Tc) decreases.The precipitated crystalline phase is β-CaO·SiO2.When fluorine and sulphur are added together to the glass,the ability of bulk crystallization increases and Tc further decreases.Either β-CaO-SiO2 or α-CaO-SiO2 precipitates depending on the heat treatment procedure.
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