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《Glass & Enamel》 2001-04
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Preparation and Characterization of Stable Zirconia Sol

ZHOU Cai?hua 1, HE Chao 1, HU Xing?fang 1, LUO Houg?jie 2, (1. R & D Center of Shanghai Institute of Ceramics, Chinese Academy of Science, Shanghai, 200050, China; 2. Department of Material Science & Engineering, Northwest Institute of Light Indust  
Zirconia film is now probably one of the most widely studied and applied inorganic films in the material research. Sol-gel process is the most useful way to prepare zirconia film. The key to this process is to obtain stabilized zirconia sol.In this paper, a method using inorganic salt (zirconia chloride octahydrate) as precursor and first using oxydol as catalyst to produce stable zirconia sol was reported. Mechanism and effect of oxydol acting on the system was studied via analyzing the influence of the ratio of H 2O 2/Zr on the relationship of sol viscosity and particle size distribution vs time. And by means of IR, XRD and TEM, the structure of the sol, phase and feature of the sol particles were studied respectively. The results showed that oxydol effectively accelerated hydrolysis of the system, the sol system was fairly stable and it was an economic and practical sol to prepare zirconia films.
【CateGory Index】: TQ427
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