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《Glass & Enamel》 2009-01
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Preparation of Glass-ceramics in Bi_2O_3-B_2O_3-WO_3 System

WANG Zhi-qiang,TONG Rui,LIN Hai,LI Chang-min,ZHOU Jie,GAO Jin-rui (School of Chemical Engineering and Materials,Dalian Polytechnic University,Dalian 116034,China)  
The matrix glasses with composition of 0.97[xBi2O3(1-x)B2O3]·0.03 WO3(0.25≤ x ≤0.75) were prepared by melting method and glass-ceramics were obtained by heat treatment at characteristic temperatures determined by DTA.The results show that only two kinds of glasses with x=0.67 and x=0.60 in all prepared matrix glasses can develop into milk yellow glass-ceramics after proper heat treatment,and their crystalline phases are BiO2 and Bi2WO6 respectively.The crystals in both glass ceramics observed under scanning electron microscope show granular in shape and their sizes are within the range of 0.8~1.0μm.The glasses in this system are characterized with higher density and lower hardness.However,density and hardness of glass-ceramics after heat treatment are higher than that of untreated glasses.
【Fund】: 辽宁省教育厅高等学校科学研究基金资助项目(05L076 20060162);; 辽宁省自然科学基金资助项目(20041067)
【CateGory Index】: TQ171.6
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