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《Journal of Jiangxi Normal University (Natural Sciences Edition)》 1994-01
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The Synthesis of ω-methylcamphene from Camphene

Xiao Zhuanquan Hu Tanxiang(Dept. of Chem. of Jiangxi Normal University,Nanchang 330027)  
This paper reports a new way for the synthesis of E ω-methylcamphene. E-ω-methylcam-phene could be synthesized by Raney nickel reduction of the dithioketal , which is prepared from camphene by Vilsmeier -Haack formylation and acetalation. The dithioketal and E-ω-methylcamphene have been purified and characterized with MS, IR and H-NMR.
【Fund】: 国家自然科学基金资助课题
【CateGory Index】: O643.3
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【References】
Chinese Journal Full-text Database 1 Hits
1 Xiao Zhuanquan Lai Chunqiu(Dept.of Chem., Jiangxi Normal University, Nanchang 330027);The Synthesis of Endo-isocamphanylchloromethane[J];Journal of Jiangxi Normal University (Natural Sciences Edition);1994-04
【Citations】
Chinese Journal Full-text Database 4 Hits
1 Zhong Ping, Jin Jinliang, Li Xicheng;Synthesis of ω-Formyl Camphene and Determination of its Configurations[J];Journal of Jiangxi Normal University(Natural Sciences Edition);1987-03
2 Xiao Zhuanquan Li Huiming (Dept.of Chem.);The Syntheses of α-isocamphanyl Alcohols and Isocamphanyl-hydrocarbyl Ketones[J];Journal of Jiangxi Normal University(Natural Sciences Edition);1992-04
3 Xiao Zhuanquan Zhong Ping Jin Jinliang Chen Jing Chen Aili (Department of Chemistry, Jiangxi Normal University Nanchang 330027);THE SYNTHESIS AND ANALYSIS OF ω-ACYLCAMPHENE COMPOUNDS AND THEIR PERFUMES[J];Chemistry & Industry of Forest Products;1992-02
4 WANG Shao-Hua ZHONG Xiang-Ju HE Jian LIANG Meng-Lan~* (Dept.of Chem.Eng.,Beijing Institute of Light Industry,Beijing);Synthesis of some Flavorous Cyclic Ketal Compounds[J];Chinese Journal of Organic cHEMISTRY;1988-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 Xiao Zhuanquan (Dept. of Chem.);Study on the Reactions of co-Formylcamphene and Its Applications to Synthesis II--Condensation Reactions with Methyl Alkyl Ketones[J];Journal of Jiangxi Normal University(Natural Sciences Edition);1992-02
2 Xiao Zhuanquan Li Huiming (Dept.of Chem.);The Syntheses of α-isocamphanyl Alcohols and Isocamphanyl-hydrocarbyl Ketones[J];Journal of Jiangxi Normal University(Natural Sciences Edition);1992-04
3 Xiao Zhuanquan He Yonghong (Dept.of Chem.);Study on the Reactions of ω-Formylcamphene and Its Uses in Synthesis Ⅲ——Catalytic Hydrogenation and Synthesis of Dihydro-ω-formylcamphene[J];Journal of Jiangxi Normal University(Natural Sciences Edition);1993-03
4 Xiao Zhuanquan Lai Chunqiu(Dept.of Chem., Jiangxi Normal University, Nanchang 330027);The Synthesis of Endo-isocamphanylchloromethane[J];Journal of Jiangxi Normal University (Natural Sciences Edition);1994-04
5 Xiao Zhuanquan Lai Chunqiu Fu Haiping(Dept. of Chem. Jiangxi Normal Univenity.Nanchang 330027);One-step Syuthesis of E ω-acetylcamphene from Camphene[J];Journal of Jiangxi Normal University (Natural Sciences Edition);1995-02
6 Xiao Zhuanquan Lai Chunqiu Li Xicheng(Dept.of Chem.,Jiangxi Normal University,Nanchang 330027);Synthesis of Endo-isocamphanylmethyl Cyanide[J];Journal of Jiangxi Normal University (Natural Sciences Edition);1995-04
7 LIU Hui 1, LI Ping 2, XU Li yan 3, XIAO Zhuan quan 2 (1.Department of Chemistry,Zhenjiang Teachers' College,Jiangsu Zhenjiang 212003,China;2.Institute of Chemistry and Biological Science,Jiangxi Normal University,Nanchag 330227,China;3.Jiangxi P;Study on Camphene Carbonacylation[J];Journal of Jiangxi Normal University (Natural Sciences Edition);2001-02
8 WU Suqin1,XIAO Zhuanquan2,PENG Lanhua2 (1.College of Sciences, Jiangxi Agricultural University, Nanchang 330045, China;2.Institute of Chemistry Sciences,Jiangxi Normal University, Nanchang 330027,China);Mass Spectra Analysis of Endo-Isocamphanyl-Hydrocarbyl Ketone Compounds[J];Journal of Jiangxi Normal University (Natural Sciences Edition);2003-03
9 LI Yan-xia~1,WEN Hong-li~2,FU Chang-qing~2,WANG Xing-cong~2,XIAO Zhuan-quan~2 (1.College of Sciences,Jiangxi Agricultural University,Nanchang 330045,China;2.Institute of Chemistry,Jiangxi Normal University,Nanchang 330027,China);Study on the Reduction of ω-Acylcamphene with Sodium in Aguous Ammonia[J];Journal of Jiangxi Normal University (Natural Sciences Edition);2004-02
10 Xiao Zhuqnquan;Zhang Xuehong;Lai Chunqiu (Department of Chemistry,Jiangxi Normal University,Nanchang 330027)Wang Xine(Jiangxi Building Materials Industry College,Nanchang 330029);Synthesis of Alkyl E-8-camphenylcarboxylic Acid Esters from Camphene[J];JOURNAL OF JIANGXI NORMAL UNIVERSITY (NATURAL SCIENCES EDITION);1996-01
【Co-references】
Chinese Journal Full-text Database 1 Hits
1 Xiao Zhuanquan He Yonghong (Dept.of Chem.);Study on the Reactions of ω-Formylcamphene and Its Uses in Synthesis Ⅲ——Catalytic Hydrogenation and Synthesis of Dihydro-ω-formylcamphene[J];Journal of Jiangxi Normal University(Natural Sciences Edition);1993-03
【Secondary References】
Chinese Journal Full-text Database 3 Hits
1 Xiao Zhuanquan Lai Chunqiu Li Xicheng(Dept.of Chem.,Jiangxi Normal University,Nanchang 330027);Synthesis of Endo-isocamphanylmethyl Cyanide[J];Journal of Jiangxi Normal University (Natural Sciences Edition);1995-04
2 Xiao Zhuanquan;Lai Lifang;Zhang Zuehong(Department of Chemistry,Jiangxi Normal University,Nanchang 330027);Synthesis of Endo-α-ethylisocamphanylformaldehyde[J];JOURNAL OF JIANGXI NORMAL UNIVERSITY (NATURAL SCIENCES EDITION);1996-02
3 Xiao Zhuanquan ① Wen Chuiyi ② Li Huiming ① Liu Hui ① Li Xichun ① (① Department of Chemistry,Jiangxi Normal University,Nanchang 330027;② Department of Basic Courses,Jiangxi Agricultural University,Nanchang 330045));Synthesis of Acetic Ester of Endo α isocamphanyl Alcohols[J];JOURNAL OF JIANGXI NORMAL UNIVERSITY (NATURAL SCIENCES EDITION);1996-03
【Secondary Citations】
Chinese Journal Full-text Database 4 Hits
1 Zhong Ping, Jin Jinliang, Li Xicheng;Synthesis of ω-Formyl Camphene and Determination of its Configurations[J];Journal of Jiangxi Normal University(Natural Sciences Edition);1987-03
2 Zhong Ping Jin Jinliang Li Xicheng ( Jiangxi Normal University Nanchang );VILSMEIER-HAACK'S FORMYLATING REACTION OF CAMPHENE AND ITS DERIVATIVES[J];Chemistry & Industry of Forest Products;1988-03
3 Lin Zhongxiang (Nanjing Forestry University Nanjing 210037) Hu Hongwen (Nanjing University Nanjing 210008);INDIRECT ω-ACYLATION OF CAMPHENE AND LONGIFOLENE[J];Chemistry & Industry of Forest Products;1991-03
4 ;ω—甲酰基莰烯的制备[J];Flavour Fragrance Cosmetics;1987-03
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