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《Journal of Jiangxi Normal University (Natural Sciences Edition)》 2004-01
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Solid State Synthesis and Characteristies of (NH_4)_3PW_6Mo_6O_(40)·8H_2O Nanoparticle

SHI Xiao-bo~(1,2),WANG Guo-ping~3,LI Chun-gen~1,WANG De-xian~1 (1.Insititute of Chemistry,Jiangxi Normal University,Nanchang 330027,China;2.Department of Chemistry,Zhanjiang Normal College,Zhanjiang 524048,China;3. School of Materials Science and Engineering,Hefei University of Technology,Hefei 230009,China)  
The polyoxometate particle (NH_4)_3PW_6Mo_6O_(40)·8H_2O were synthesized by solid-state reaction at room temperature. Their structure, particle size, thermal properties and surface nature were characterized with elemental analyses, IR, XRD, TEM, TG-DTA and BET techniques. The results show that the polyoxometate particle (NH_4)_3PW_6Mo_6O_(40) are found to exhibit Keggin structure, have a surface area of 134.2 m~2·g~(-1), the mean grain size is 12 nm,the stability of the hetoropoly anion decreased when nanoparticles were formed.
【Fund】: 国家自然科学基金资助项目(20261003).
【CateGory Index】: O614
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