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《Journal of Jiangxi Normal University (Natural Sciences Edition)》 2005-04
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Synthesis and Identification of the Dimethybis(phenylmethyl)silane

YE Shang-hui, SONG Cai-sheng, FU Chang-qing, LIU Yong-jun, LIU Xiao-ling(Insitute of Chemitry and Chemical Engineering Sciences,Jiangxi Normal University, Nanchang 330027,China)  
A reactive silicate monomer dimethy bis(phenylmethyl)silane(DMDPMS) was prepared by dichlorodimethylsilane and phenyl methyl chloride, in the present of Mg, and was analyzed and identified by FT-IR,(~1 H NMR,)~(13) C NMR and melting-point.The effect of the process, solution and concentration on the purity and productivities of the product was studied, which results show that the using phenylmethyl chloride as alkylation reagent,THF as solution,whose concentration is 1.25 mol/L,and the "novel process" was better for the preparation of DMDPMS, whose melting point was 57~58 ℃, compared with normal process .
【Fund】: 国家“863”计划(2002AA333120);; 国家自然科学基金(20264001)资助项目
【CateGory Index】: TQ264.1
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