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The Synthsis of Indanone-[1]-Thiosem Icarbazone-5,6-Benzo-18-Crown-6

ZHANG Lai-xin,YANG Qiong (Department of Chemistry and Chemical Engineering,Baoji College of Arts and Sciences,Baoji Shanxi 721007,China)  
Indanone-[1]-5,6-benzo-18-crown-6 has been synthesized by acylation in polyphosphoric acid(PPA),it was then reacted with thiosemicarbazide under acid condition to give indanone-[1]-thiosemicarbazone and semicarbazone-5,6-benzo-18-crown-6.The two new products were characterized by elemental analysis,IR and mass spectrometry.
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