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The CdS Hollow Hemispheres:Mixed-Solvothermal Synthesis,Characterization and Optical Properties

SHEN Xiao-jie,ZHANG Lin-fei,WANG Lei,ZHONG Sheng-liang*(College of Chemistry and Chemical Engineering,Jiangxi Normal University,Nanchang Jiangxi 330022,China)  
In this work,novel cadmium sulfide(CdS) hollow hemispheres were successfully prepared via an oxalic acid-assisted solvothermal route the first time.The as-prepared products were characterized by X-ray powder diffraction(XRD),scanning electronic microscope(SEM) and transmission electron microscopy(TEM).Results show that the morphologies of the products are dependent on the reaction time and temperature.The optical properties and possible formation process for the CdS hollow hemisphere were investigated.
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