Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Chongqing University of Technology(Natural Science)》 2015-01
Add to Favorite Get Latest Update

EPI Scan Mode Screening and Identify Antibiotic Residual in Animal Products

JIN Yan;LI Xiao-dong;LIU Yu;JIANG Shi;JIANG Ling-ling;ZHOU Jian-nan;ZHENG Chen;Shenyang Enter Exit Inspection and Quarantine Bureau;AB SCIEX Asia Pacific Application Support Center;  
A method based on chromatography-tandem mass spectrometry for the simultaneous determination of 43 antibiotics in animal products with hollow cellulose membrane level PES was established. The method was developed on EPI scan mode. And a new Qtrap system was used to identifythe compound with EPI spectrometry with data library. This process was proved on excluding the false positive samples and the identification of the purity of chromatogram effectively. The standard curves are linear in concentration range of 0. 5 ~ 50 ng / m L( r 0. 99). The average recoveries are between69. 3% and 102. 4%,under the addition lever 1,5,10 μg / kg. The detection limit of the method is from 0. 2 μg / kg,and the limit of quantification is 0. 5 μg / kg. The method was applied for the qualitative and quantitative determination of 43 antibiotic residues in animal products simultaneously,and the method was proved to be rapidly,accurate and of high sensitivity characteristics. It can meet the requirement of monitoring veterinary daily analysis.
【Fund】: 国家质检总局科技计划项目(2011IK215 2014IK129);; “十二五”国家科技支撑计划项目(2011BAK10B04-9);; 辽宁省出入境检验检疫局科技计划项目(LK33-2007)
【CateGory Index】: S859.84
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 10 Hits
1 Huang Zhiyong,Cai Hongji,Huang Gaoling,Peng Aihong(College of Bioengineering,Jimei University,Xiamen,Fujian,361021);Determination of tetracycline antibiotic residucs in aquiculturc products by HPLC[J];Fujian Analysis&Testirg;2005-01
2 GUO De-Hua1,DENG Xiao-Jun* 1,ZHAO Shan-Zhen1,ZHU Jian1,XIA Chong-Fei2,CHEN Shun-Sheng2,SONG Yue3 1 ( Shanghai Entry-Exit Inspection and Quarantine Bureau,Shanghai 200135) 2 ( Shanghai Fishery University,Shanghai 200433) 3 ( China Pharmaceutical University,Nanjing 211198);Simultaneous Determination of 76 Veterinary Drug Residues in Foodstuffs of Animal Origin by Solid Phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2010-03
3 WANG Ning,ZHANG Xin-rui,CHEN Hai-qin,ZHENG Yi-min (School of Pharmacy and Bioengineer, Chongqing University of Technology,Chongqing 400054,China);Isolation and Purification of Lignans from Aritium lappa L.by Preparative HPLC[J];Journal of Chongqing University of Technology(Natural Science);2013-05
4 GUO Jie;ZHANG Chao-fei;GAO Geng-qu;MA Guang-hui;MA Wei;State Food Safety Inspection Scientific Research Center of Henan Quality Polytechnic;;Research Progress on Determination of Residues of Antibiotic in Milk by High Performance Liquid Chromatography-tandem Mass Spectrometry[J];China Animal Husbandry & Veterinary Medicine;2014-01
5 NA Guang-shui1,ZHOU Chuan-guang1,WANG Zhen1,WANG Qiang1,LI Hong-xia2,CHEN Tong3,ZHANG Yue-mei3,YAO Zi-wei11.National Marine Environmental Monitoring Center,Dalian 116023,China2.College of Life Science and Technology,Dalian Fisheries University,Dalian 116023,China3.College of Biological & Food Technology,Dalian Polytechnic University,Dalian 116034,China;Simultaneous Determination of Fifteen Sulfonamide Residues in Macrobenthos by High-Performance Liquid Chromatography Tandem Mass Spectrometry[J];Research of Environmental Sciences;2009-04
6 YANG Liu1,ZHU Jie-li1,WU Cui-rong,LU Jun1, CHAI Zhen-lin1,ZHOU Li-xiong2 (1.Zhejiang Forestry Product Test Station,Hangzhou 310023,China;2.Jiangshan Forestry Institute,Jiangshan 323700,China);Determination of Forchlorfenuron in Myica rubra by Matrix Solid Phase Dispersion Extraction and Reversed High Performance Liquid Chromatography[J];Acta Agriculturae Universitatis Jiangxiensis;2013-02
7 LIN Weixuan,DONG Weifeng,CHEN Xi,TIAN Miao,YU Ling,ZHAO Jinghong,YANG Chunguang(Liaoning Entry-Exit Inspection and Quarantine Bureau,Dalian 116001,China);Determination of hormone multi-residues in animal tissues by gas chromatography-mass spectrometry[J];Chinese Journal of Chromatography;2009-03
8 TIAN Miao(Liaoning Entry-Exit Inspection and Quarantine Bureau,Dalian 116001,China);Determination of β-Agonists Residue in Pork Tissues by Gas Chromatography-Mass Spectrometry[J];Journal of Instrumental Analysis;2010-07
9 JI Cai-ni,YUE Zhen-feng,XIE Li-qi,ZHENG Wei-ping,CHEN Pei-jin (Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen 518067,China);Study on simultaneous detection of 7 tetracyclines residues in aquatic products by high performance liquid chromatography[J];Chinese Journal of Veterinary Science and Technology;2005-10
10 XING Jin,FENG Yu-fang,YUE Bing-fei,HE Zheng-ming(Department of Laboratory Animal Quality Testing,National Institutes for Food and Drug Control,Beijing 100050,China);Antibiotic residue monitoring in laboratory animal serum by microbial inhibition test[J];Chinese Journal of Comparative Medicine;2013-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 YU Xiang-man1,ZHANG Qi-zhong1,YE Bo-xi1,Chen Guo-quan2,Gan An-hui2,ZHU Ze-yao1 (1.Institute of Hydrobiology,Jinan University,Guangzhou 510632;2.Agrotechnical Popularization Center of Baiyun District in Guangzhou 510405);Pharmacokinetics of Oxytetracycline in Hybrid Tilapia(Oreochromis aureus×O.niloticus)[J];Freshwater Fisheries;2009-01
2 WANG Bing1, SUN Cheng1, HU Guan-jiu2 (1. College of Environment and State Key Lab of Pollution Control and Resources Reuse, Nanjing University, Nanjing 210093; 2. Environmental Monitoring Center of Jiangsu Province, Nanjing 210036);Residue Antibiotics in Environment: Potential Risks and Relevant Studies[J];Environmental Science & Technology;2007-03
3 Yue Zhenfeng~(*1),Qiu Yueming~(2),Lin Xiuyun~(1),Ji Caini~(1) ~1(Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection & Quarantine Bureau of the People′s Republic of China,Shenzhen 518067) ~2(Institute of Inspection Technology and Equipment,Chinese Academy of Inspection and Quarantine,Beijing 100025);Determination of Multi-Residues of Tetracyclines and Their Metabolites in Milk by High Performance Liquid Chromatography-Tandem Positive-ion Electrospray Ionization Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2006-09
4 WANG Lian*1,LI Yuan-Qian2,WANG Hai-Bo3,GUAN Yan-Li3 1(Chengdu Center for Disease Control and Prevention,Chengdu 610041) 2(West China School of Public Health,Sichuan University,Chengdu 610041) 3(Sichuan Monitoring Center for Veterinary Drug Residue,Chengdu 610041);Simultaneous Determination of Twenty Veterinary Drug Residues in Milk and Meat Using Matrix Solid Phase Dispersion-Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2011-02
5 ZHAO Shan-Zhen1,DENG Xiao-Jun1,PENG Tao2,YI Xiong-Hai1, GUO De-Hua1,HAN Li1,SHENG Yong-Gang1,WU Qiao-Bin3 1(Shanghai Entry-Exit Inspection and Quarantine Bureau,Shanghai 200135) 2(Chinese Academy of Inspection Quarantine,Beijing 100025) 3(Shanghai Ocean University,Shanghai 200433);Determination of L-Hydroxyproline by Hydrophilic Interaction Chromatography Coupled Tandem Quadrupole Linear Ion Trap Mass Spectrometry in Protein Contained Food[J];Chinese Journal of Analytical Chemistry;2011-09
6 LUO Hui-Tai,HUANG Xiao-Lan,WU Hui-Qin,ZHU Zhi-Xin,HUANG Fang,LIN Xiao-Shan(Guangdong Provincial Public Laboratory of Analysis and Testing Technology, China National Analytical Center(Guangzhou),Guangzhou 510070);Simultaneous Determination of 33 Medicine Residues in Aquatic Products by Rapid Resolution Liquid Chromatography-Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2012-02
7 Fu Ruo-nong(Depertment of Chemistry,Beijing Institute of Technology);The advances of gas chromatography in recent two years[J];Chinese Journal of Analysis Laboratory;2011-05
8 GAO Hui1,2,ZU Guo-ren1,GU Jia1,2,CHEN Tong1,2,FANG Xiao-dan1,2,LI Yong-dong1,2 and NA Guang-shui2(1.School of Biological Technology,Dalian Polytechnic University,Dalian 116034;2.National Marine Environmental Monitoring Center,Dalian 116023);Simultaneous determination of quinolone antibiotics and estrogens in environmental water samples using high performance liquid chromatography tandem mass spectrometry[J];Chinese Journal of Analysis Laboratory;2011-12
9 Lin Ling,Zhang Chenghui,Cheng Shenghua,Zha Yubin,Yang Chunliang(Agriculture Products Processing Research Institute,Chinese Academy of Tropical Agriculture Science,Zhanjiang,524001);HPLC determination of residues of oxytetracycline,tetracycline,and chlortetracycline in pig liver[J];Analytical Instrumentation;2009-02
10 HAN Rong-wei1,3,WANG Jia-qi1,2,ZHENG Nan1,XU Xiao-min2,ZHEN Yun-peng2,QU Xue-yin2,ZHAO Lian-sheng1(1.State Key Laboratory of Animal Nutrition,Institute of Animal Sciences,Chinese Academy of Agricultural Sciences,Beijing 100193,China;2.Quality and Inspction Center of Milk and Milk Products(Beijing),Ministry of Agriculture,Beijing 100193,China;3.College of Food Science and Engineering,Qingdao Agricultural University,Qingdao 266109,China);Main Risk Factor Analysis for Milk Quality and Safety Ⅲ.Veterinary Drug Residues[J];China Animal Husbandry & Veterinary Medicine;2012-04
China Proceedings of conference Full-text Database 2 Hits
1 XU Cheng-gang 1*,WANG Jun 2,SHI Wen-chun 1,CONG Wei-hong 1,CUI Jia 1,LI Da-shuan 1,ZHOU Chang-peng 1 (1.Weihai Entry-Exit Inspection and Quarantine Bureau,Weihai 264205,China;2.Shandong Entry-Exit Inspection and Quarantine Bureau,Qingdao 266001,China);Determination of 3 β-agonists Residues in Pork by High Performance Liquid Chromatography-Tandem Mass Spectrometry[A];[C];2012
2 Zhuo Chen;Jun Chen;Li Xu;Beijing Institute of Microchemistry;;Mental Drugs Analysis in Swine Tissues[A];[C];2014
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 LI Rui-juan1,YU Jian-lei1,SONG Guo-chun1,SHAO Yu-jie2(1.Plant Protection Institute of Shandong Academy of Agricultural Sciences,Jinan 250100,China;2.Penglai Agricultural Bureau,Penglai 265600,China);Degradation Dynamic and Residue Determination of Forchlorfenuron in Chinese Goosebeery Fruit and Soil[J];Shandong Agricultural Sciences;2009-02
2 LIU Qiang 1, 2 , GONG Daoxin 1 * , PENG Xiaochun 2 , and YAN Xiaojun 1 1 College of Resources and Environment, Hunan Agricultural University, Changsha 410128, China 2 South China Institute of Environmental Science, Ministry of Environment Protection, Guangzhou 510655, China;Determination of Forchlorfenuron Dissipation and Residue in Cucumbers and Red Soil[J];东北农业大学学报(英文版);2010-01
3 YE Sai1,2,ZHANG Kui-wen2,3,YAO Zi-wei2,MA De-yi2(1.College of Environmental Science and Engineering,Dalian Maritime University,Dalian 116026,China;2.Coastal Ecology Key Laboratory,National Marine Environmental Monitoring Center,Dalian 116023,China;3.School of Life Science and Technology,Dalian Fisheries University,Dalian 116023,China);Occurrence of sulfonamide pharmaceuticals in water column around Bohai sea[J];Journal of Dalian Maritime University;2007-02
4 Wu Qian Zheng Jing Huang Xiaorong Chen Bin Lin Jie (Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou 350001 China);Residue Analysis of β-Lactams Antibiotics Drugs in Animal Derived Food by Microbiological inhibition assay[J];Fujian Journal of Animal Husbandry and Veterinary Medicine;2009-02
5 WANG Bing1, SUN Cheng1, HU Guan-jiu2 (1. College of Environment and State Key Lab of Pollution Control and Resources Reuse, Nanjing University, Nanjing 210093; 2. Environmental Monitoring Center of Jiangsu Province, Nanjing 210036);Residue Antibiotics in Environment: Potential Risks and Relevant Studies[J];Environmental Science & Technology;2007-03
6 ZHANG Lan, LIN Zi-an, XIE Zeng-hong(Department of Chemistry, Fuzhou University, Fuzhou 350002, China);Simultaneous Determination of Five Residual Antibioticsin Seafood by Capillary Electrophoresis[J];Analysis and Testing Technology and Instruments;2004-01
7 YU Jian-xin,HU Xiao-zhong,YU Chun,LIN Yan-fei,LI Ya-fei,YANG Zhi-xue,YAN Yi,WANG Peng,LI Jing,ZHANG Li(Technology Center of Hubei Entry-Exit Inspection and Quarantine Bureau,Wuhan 430022,China);High-Performance Liquid Chromatography-Tandem MassSpectrometry for the Determination of β-Agonist[J];Analysis and Testing Technology and Instruments;2004-04
8 Wang Lei, Xu Zhixiu, Zhang Xiaosong, Shao Xueguang * (Department of Chemistry, University of Science and Technology of China, Hefei 230026);Rapid Determination of 7 Tetracyclines by Reversed Phase High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2003-01
9 Yue Zhenfeng~(*1),Qiu Yueming~(2),Lin Xiuyun~(1),Ji Caini~(1) ~1(Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection & Quarantine Bureau of the People′s Republic of China,Shenzhen 518067) ~2(Institute of Inspection Technology and Equipment,Chinese Academy of Inspection and Quarantine,Beijing 100025);Determination of Multi-Residues of Tetracyclines and Their Metabolites in Milk by High Performance Liquid Chromatography-Tandem Positive-ion Electrospray Ionization Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2006-09
10 Wu Yinliang ~ 1,2 , Liu Suying~ 2 , Liu Yongjun~ 2 ,Shen Jianzhong~ *1 , Wang Hai~ 2 , Shan Jihao~ 2 ~ 1 (College of Veterinary Medicine, China Agricultural University, Beijing 100094) ~ 2 (Quality Control and Inspection Center for Domestical Animal Products of Ministry of Agriculture, Beijing 100026);Determination of Residual Salbutamol in Swine Tissue by Solid Phase Extraction with Gas Chromatography-Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2006-S1
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved