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《Materials Review》 2014-16
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Preparation,Structure and Properties of Blend Films of Feather Keratin and Sodium Carboxy Methyl Cellulose

WANG Haiyang;YIN Guoqiang;FENG Guangzhu;DOU Yao;HE Ming;DENG Xiangwen;Green Chemical Institute,Zhongkai University of Agricultural Engineering;  
Blend films based on hydrolysis of feather keratin and sodium carboxy methyl cellulose,compatibilized by glycerol,were prepared by solution casting.Infrared spectroscopy(FTIR-ATR),X-ray diffraction(XRD),differential scanning calorimetry(DSC),thermogravimetry analysis(TG)and scanning electron microscopy(SEM)were employed to characterize the structure and properties between FK and CMC in the blending systems.FTIR showed that Maillard reactions occurred between CMC and FK,and XRD results indicated that the addition of CMC destroyed the crystal structure of the FK,the blend films generated new crystallizations by Maillard reaction,while addition of glycerol also reduce the crystallinity of the blend films.According to DSC analysis,FK/CMC blends had a singleglass transition temperature(Tg)between 110℃and 160℃,indicating that CMC and FK has good compatibility.TG results indicated that addition of CMC enhanced thermal stability of the blend films.
【Fund】: 国家自然科学基金(21176269);; 广东省自然科学基金(9251022501000003);; 广东省高校科技创新项目(2013KJCX0102);; 仲恺农业工程学院学生创新基金(201312)
【CateGory Index】: TQ321.4
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