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《Chinese Journal of Luminescence》 2003-01
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Preparation and Photoluminescent Property of Polymeric Dis(8-hydroxyquinoline schiff base) Zinc Complexes

TAN Song-ting, ZHOU Jian-ping, ZHAO Bin, PENG Jun-hua (Institute of Polymer Materials, Xiangtan University, Xiangtan 411105, China)  
Three different ligands with bis(8-hydroxyquinoline) were prepared by nucleo-philic addition reaction between 5-formyl-8-hydroxyquinoline and three diamines (4, 4′-phenylenediamine, 4,4′-biphenyl-diamine and 4,4′-diamina-diaphenyl sulfone). Then these ligands were coordinated with zinc ion to prepare three new polymeric bis(8-hydroxyquinoline schiff base) zinc complex. The chemical structure of ligands and complexes was characterized by infrared absorption spectroscopy, ultraviolet absorption spectroscopy and elemental analysis, the results indicated that it was just the object we wanted. The photoluminescent performance of these complexes were investigated by fluorescence, the results showed that strong fluorescent emission peaked between 425nm and 625nm when excited by the light of maximal excitation wavelength, the peaks are at 497, 499 and 499nm for complex Zn-DD8Q, Zn-PD8Q and Zn-DDS8Q respectively, which is between blue light and green light. The fluorescence intensity of complex Zn-DD8Q is stronger in comparison with complex Zn-PD8Q and Zn-DDS8Q, due to DD8Q has stronger conjugative effect. It means the fluorescence intensity is changed by chemical structure of complex. When conjugative effect bigger, the fluorescence stronger. In general, a kind of excellent EL material may be also a kind of eminent PL material. So, the research object of EL material can be extended from the excellent PL material. Hence, in this research work we study the material′s PL performance and make setout for the next research of EL materials.
【Fund】: 教育部基金 ( 0 10 83) ;; 湖南省教育厅重点项目 ( 0 1A0 0 2 );; 湖南省自然科学基金 ( 0 0JJY2 0 12 )资助项目
【CateGory Index】: TN383
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