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《Chinese Journal of Luminescence》 2012-12
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Hydrothermal Synthesis of Morphology Controllable ZnMoO_4 Microcrystal and Its Photoluminescence Property

LV Wei1,LIU Xuan1,WU Li-li2,LIU Xin1(1.School of Chemistry and Chemical Engineering,Shandong University,Ji'nan 250100,China; 2.School of Materials Science and Engineering,Shandong University,Ji'nan 250061,China)  
ZnMoO4 microcrystals with diffrent morphologies and structures have been successfully prepared via hydrothermal method using Zn(Ac)2 and(NH4)6Mo7O24·4H2O.In the synthesis process,cetyltrimethyla-mmonium bromide(CTAB),sodium dodecyl sulfate(SDS),polyvinyl pyrrolidone-K30(PVP-K30) and ethylene diamine tetraacetic acid(EDTA) were added,respectively.XRD,SEM,photoluminescence(PL) were used to characterize the as-obtained ZnMoO4 microcrystals.The results suggest that the morphologies and structures of ZnMoO4 microcrystal can be controlled by changing the type and dosage of the adjuvant or varying the reaction time,the luminous intensity of the samples are different and the luminous center are all around 565 nm.
【Fund】: 山东省自然科学基金(Y2008G25);; 济南市高校自主创新项目(200815063 201102058)资助项目
【CateGory Index】: TB383.1
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