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《Chinese Journal of Luminescence》 2015-01
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Synthesis of Naphthalimide Derivatives and Its Recognition for Picric Acid

YU Ying-hao;DU Bin;DING Zhi-jun;WANG Pu-hong;GUO Lei;YU Jian-hua;HU Yu-lai;Department of Chemistry and Chemical Engineering,Northwest Normal University;Research Institute of Chemical Defense;  
N-hexyl-4-[2-(3-phenyl-thiourea)-ethylamino]-naphthalimide(HTN),a naphthalimide derivative,was synthesized and its structure was determined by NMR and MS. The recognition of HTN for picric acid(PA) was investigated by fluorescence spectrum. The results show that the fluorescence intensity of HTN significantly reduces with the increasing of PA concentration in C2H5 OH /H2O(2∶ 1). For PA concentration from 1 × 10- 6mol·L- 1to 5 × 10- 4mol·L- 1,the quenching rate,(I0- I)/I0,correlates linearly with [PA]0. 5,and R2= 0. 995 5. Meanwhile,no obvious interference is observed in the presence of the benzene series such as aniline,benzaldehyd,trinitrotoluene,phenol,styrene,pyridine,p-toluenesulfonic acid,toluene,nitrobenzene and chlorobenzene,indicating HTN's excellent selectivity and high sensitivity for the detection of PA.
【Fund】: 国家重点基础研究发展计划(973)(2011CB706902);; 国家重大科学仪器设备开发专项(2011YQ150078);; 国家自然科学基金(21262031)资助项目
【CateGory Index】: O625.6
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