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《Chinese Journal of Luminescence》 2015-01
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Synthesis of Naphthalimide Derivatives and Its Recognition for Picric Acid

YU Ying-hao;DU Bin;DING Zhi-jun;WANG Pu-hong;GUO Lei;YU Jian-hua;HU Yu-lai;Department of Chemistry and Chemical Engineering,Northwest Normal University;Research Institute of Chemical Defense;  
N-hexyl-4-[2-(3-phenyl-thiourea)-ethylamino]-naphthalimide(HTN),a naphthalimide derivative,was synthesized and its structure was determined by NMR and MS. The recognition of HTN for picric acid(PA) was investigated by fluorescence spectrum. The results show that the fluorescence intensity of HTN significantly reduces with the increasing of PA concentration in C2H5 OH /H2O(2∶ 1). For PA concentration from 1 × 10- 6mol·L- 1to 5 × 10- 4mol·L- 1,the quenching rate,(I0- I)/I0,correlates linearly with [PA]0. 5,and R2= 0. 995 5. Meanwhile,no obvious interference is observed in the presence of the benzene series such as aniline,benzaldehyd,trinitrotoluene,phenol,styrene,pyridine,p-toluenesulfonic acid,toluene,nitrobenzene and chlorobenzene,indicating HTN's excellent selectivity and high sensitivity for the detection of PA.
【Fund】: 国家重点基础研究发展计划(973)(2011CB706902);; 国家重大科学仪器设备开发专项(2011YQ150078);; 国家自然科学基金(21262031)资助项目
【CateGory Index】: O625.6
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【Citations】
Chinese Journal Full-text Database 5 Hits
1 CHEN Jie1,HE Ying1,PAN Zhao-dong1,ZHANG Yao-fei1,ZHU Di1,GU Ying1,WANG Jun-an2(1.Department of Polymer Materials,School of Materials Science & Engineering,Shanghai University,Shanghai 200072,China; 2.Institute of Materials,School of Materials Science and Engineering,Shanghai University,Shanghai 200072,China);Synthesis and Optoelectronic Properties of Aromatic Polyethers with A 1,8-naphthalimide Unit Main Chain[J];Chinese Journal of Luminescence;2012-03
2 ZHAO Hong-shuai,CHANG Miao,LIU Bao-xian,ZOU Ben-dong Beijing Municipal Environmental Monitoring Centre,Beijing 100044,China;Quickly Determination of Pricia Acid in Water By High Performance Liquid Chromatography[J];Environmental Monitoring in China;2013-04
3 Cui Fangyun;Zhou Peng;Wang Weimin;Jin Chaoxi;Nie Hongna;Luoyang Environment Monitoring Sation;Nuclear Power Engineering Co. Ltd;Chemical Engineering and Pharmaceutics College,Henan University of Science and Technology;;Progress of Methods for Determination of Picric acid in Water[J];Northern Environment;2013-07
4 SHI Yan-ju;MA Yu-xia;CHUI Min;DU Yuan-jiang;XIE Fei;Inner Mongolia Environment Monitoring Station;;Determination of Picric Acid by Gas Phase Chromatography[J];Inner Mongolia Petrochemical Industry;2014-07
5 TIAN Juan;CHEN Biao;L Hao;WU Zhi-bing;Center for Research and Development of Fine Chemicals,Guizhou University;;Progress in fluorescence resonance energy transfer probes for detection of cation ions based on 1,8-naphthalimide-rhodamine dyads[J];Applied Chemical Industry;2014-02
【Co-citations】
Chinese Journal Full-text Database 2 Hits
1 SHI Yan-feng;PU Xue-wei;LI Guo-wen;SHAO Ying-chun;Yuxi City Environmental Monitoring Station.;;Determination of picric acid in water by direct injection-liquid chromatography /tandem mass spectrometry[J];Chinese Journal of Analysis Laboratory;2014-08
2 WANG Peng;ZHANG Guang-hua;XIANG Rui;FU Xiao-long;MOE Key Laboratory of Additives Chemistry & Technology for Light Chemical Industry,Shaanxi University of Science &Technology;;Synthesis of Coumarin Light Stabilizer Containing the Structure of Benzophenone and Its Applications[J];Fine Chemicals;2014-02
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Guan Lifeng(Taizhou City Water Company,Taizhou 225300,China);Determination of Picric Acid in Water[J];Environmental Science and Management;2008-02
2 CHEN Yong,LV Gui-bin,FAN Li(Chengdu Environmental Monitoring Centre,Chengdu 610072,China);Determination of Picric Acid in Water by Liquid Chromatography-Mass Spectrum[J];Environmental Science & Technology;2011-S1
3 He Xingcun Cai Yaqi Hu Zhide (Department of Chemistry,Lanzhou University);FLOTATION OF AQUA-CATION OF RHODIUM(Ⅲ) BY SODIUM DODECYLBENZENE SULFONATE AND SEPARATION OF RHODIUM(Ⅲ) FROM PALLADIUM(Ⅱ) AND PLATINUM(Ⅳ)[J];Chinese Journal of Analytical Chemistry;1989-04
4 Shen Aibao; Zhang Zhujun(Deparlment of Chemistry , Shaanxi Normal University, Xi' an 710062);Determination of Picric Acid Based on Fluorescence Quenching of 4-Methylumbelliferone[J];Chinese Journal of Analytieal Chemistry;1996-05
5 Long Liping 1, Wang Kemin 2, Yang Ronghua 2, Yang Xiaohai 2 1 (Department of Chemistry & Environmental Engineering, Hunan City College, Yiyang 413049) 2 (College of Chemistry & Chemical Engineering, Hunan University, Changsha 410082);A Picric Acid Optical Chemical Sensor Based on Fluorescence Quenching[J];Chinese Journal of Analytical Chemistry;2003-04
6 WANG Shu-min,FAN Xue-mei,BAI Xiao-jing,CHEN Feng-ying and WANG Xian-sheng(Department of Chemistry and Chemical Engineering,Shangluo University,Shangluo 726000);Potassium permanganate-glyoxal chemiluminescence system for determination of picric acid[J];Chinese Journal of Analysis Laboratory;2011-08
7 YE Peng-fei1,LIU Lei2,HE De-wen2,LIANG Ding-min2(1.Huizhou Environmental Protecting Bureau,Huizhou Guangdong 516001,China;2.Department of Environmental Engineering,Central South University,Changsha Hunan 410083,China);Determination of Picric Acid extracted with dichloromethane in Water by GC-MSD[J];Arid Environmental Monitoring;2010-02
8 JIANG Fang-Minga,b DAI Feic TAN Ai-Xia HUANG Zhi-QiangaZHANG Yinga ZHOU Fang-Qinca(Hunan Exit-Entry Inspection and Quarantine Bureau,Changsha 410004,P.R.China)b(College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,P.R.China)c(College of Chemistry,Xiangtan Universty,Xiangtan,Hunan 411105,P.R.China);Determination of Picric Acid in Pyrotechnic Composition by High Performance Liquid Chromatography[J];Chinese Journal of Spectroscopy Laboratory;2011-03
9 Xie Fuqing; He Xingcun; Jiang Yimin (Wuzhou Teachers’College,Babu,Guangxi,542800)(Department of Chemistry,Guangxi Normal University,Sanlidian,Guilin,541004);Flotation-SpectrophotometricDetermination of Trace Picric Acid in Water[J];GUANGXI SCIENCES;1994-04
10 WEI Jin-jin(Nanning Environmental Protection Monitoring Station,Nanning,Guangxi,530012,China);Study on the Optimal Method for Determination of Picric Acid in Water[J];Journal of Guangxi Academy of Sciences;2011-02
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