Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Environmental Science & Technology》 2010-01
Add to Favorite Get Latest Update

Determination of Phthalates in Plastic Toys by High Performance Liquid Chromatography

CHEN Zhu-ling,CHEN Fei,LIN Xiang-cheng,HUANG Yu-kui(School of Chemistry and Chemical Engineering,Fuzhou University,Fuzhou 350002,China)  
High performance liquid chromatography method was developed for rapid separation and determination of 5 kinds of phthalates(phthalic acid esters)in plastic toys.A separation was performed on a shim-pack VP-ODS column with 4.6mm× 150mm,5μm and CH3OH:H2O(V/V 90:10)with a flow rate of 1.0mL/min as mobile phase and detection wavelength 230nm.Calibration curve was linear in the concentration range of 0.5~1,000mg/L,LOD 0.34~0.96μg/L and mean recovery ranged from 93.00% ~105.23% .The method was used to analyze phthalates in different plastic toys under the optimized conditions of the extraction and purification of samples,with satisfactory results.
【Fund】: 福建省教育厅科研项目资助(JA05185)
【CateGory Index】: TS958.07
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 4 Hits
1 Wei Aixue Xu Xiaobai(Research Center for Eco-Environmental Sciences,Chinese Academy of Sciences,Beijing 100085);Research on the pollution of phthalate esters compounds in the environment[J];Techniques and Equipment for Environmental Pollution Control;2005-07
2 QIU Dong ru,WU Zhen bin, HE Feng (State Key Laboratory of Freshwater Ecology and Biotechnology,Institute of Hydrology,CAS, Wuhan 430072,China);Effects of Endocrine Disrupting Chemicals on Animals and Mechanisms of Action[J];RESEARCH OF ENVIRONMENTAL SCIENCES;2000-06
3 LIN Xing-tao, WANG Xiao-yi, CHEN Ming, REN Ren (College of Environmental and Energy Engineering, Beijing University of Technology, Beijing100022, China);Analysis of Phthalic Acid Esters of Environmental Hormone in Water Using Solid Phase Extraction and High Performance Liquid Chromatography[J];Research of Environmental Sciences;2004-05
4 Jia Li, Xia Min, Chen Hui#(Beijing Center for Physical and Chemical Analysis,Beijing 100089; #Capital Normal University , Beijing 100037);Determination of Phthalates in Plastics by High Performance Liquid Chromatography[J];Chemistry;2005-12
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 CHEN Ji-an1,QIU Zhi-qun1,SHU Wei-qun1,CAO Jia2(1.Department of Environmental Hygiene,Faculty of Preventive Medicine,Third Military Medical University,Chongqing 400038;2.Department of Military Toxicology,Faculty of Preventive Medicine,Third Military Medical University,Chongqing 400038,China);Pollution of PAEs in Water and the Biodegradations Studies in China[J];Carcinogenesis,Teratogenesis & Mutagenesis;2007-03
2 YUAN Jun-wei et al (Tianjin University of Science and Technology, Tianjin 300457);Transfer of Plasticizer DOP from PVC Film and Diversify Rule of Film Property[J];Journal of Anhui Agricultural Sciences;2006-08
3 Wang Peihua 1 (1.Suihua College, Suihua 152061);Environmental Hormones and Their Harmful Effects[J];North Environment;2005-02
4 Chen Bo1,2,Lin Jianguo1,Chen Qing1(1.LiuZhou Vocational Technical College,Liuzhou 545006,China; 2.School of Environment Science and Technology,TianJin University,Tianjin 300072,China);Research on Contamination of Phthalate Esters in Aqueous Environment and Its Environmental Behaviors[J];Environmental Science and Management;2009-02
5 Luo Guyuan1,Li Ping1,Xu Xiaoyi1,Liang Yan1,Cai Wenliang1,Du Xian1,Cao Jia2,Shu Weiqun2(1.Faculty of Urban Construction and Environment Engineering,Chongqing University,Chongqing 400045,China;2.Third Military Medical University,Chongqing 400030,China);Distribution Characteristics and Ecological Security Assessment of Phthalic Acid Esters in Wet Season in the River Basins of Main Districts of Chongqing[J];Environmental Science and Management;2009-04
6 ZHENG Xiao-ying, ZHOU Yu-wen (College of Architecture and Civil Engineering, Beijing University of Technology, Beijing 100022, China);Study on Phthalate Esters in Beijing Sewage Sludges[J];Journal of Beijing University of Technology;2006-04
7 CHEN Zhao-qiong1,YAN Pin2,LI Mao-quan1,WEI Min1,CHEN Wei-zhong(1.Department of Public Health,Chengdu Medical College,Chengdu 610083,China;2.College of Chemistry and Environmental Protection Engineering,Southwest University for Nationalities,Chengdu,610041);The Research Progress in Analysis Methods of Phthalate Easters[J];Journal of Chengdu Medical College;2007-01
8 SU Xiao-dong1,2,JIA Yun1(1.College of Chemistry and Chemical Engineering,Chongqing University of Science and Technology,Chongqing 400042,China;2.College of Chemical Engineering,Sichuan University,Chengdu 610065,China);Progress in application of high performance liquid chromatography in determining content of hormones in cosmetics[J];China Surfactant Detergent & Cosmetics;2008-03
9 CHEN Xi,SUN Ji-chao,HUANG Guan-xing,LIU Jing-tao (Institute of Hydrogeology and Environmental Geology,Chinese Academy of Geological Sciences,Shijiazhuang 050061,China);Advance of Research on Phthalate Esters Pollution and its Harmfulness[J];Ground Water;2008-02
10 LIN Xing-tao,CHEN Ming, WANG Xiao-yi, ZHANG Shu-fen, WU Shao-hua, CHEN Sha, WANG Gui-hua, REN Ren (College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100022);Analysis of Phthalate Esters of Environmental Hormone in Water Samples of Wastewater Treatment Plant[J];Environmental Science and Technology;2004-06
【Secondary Citations】
Chinese Journal Full-text Database 5 Hits
1 LIU Zhen ling  , LI Cong hui (Department of Chemistry,Xinxiang Medical College,Xinxiang 453003) and WU Cai ying (Department of Chemistry, Wuhan University,Wuhan 430072);Determination of di-(2-ethyl)hexyl phthalate in immersed plastic solution by solid phase microextration and gas chromatography[J];Analytical Laboratory;2002-01
2 QIU Dong ru,WU Zhen bin, HE Feng (State Key Laboratory of Freshwater Ecology and Biotechnology,Institute of Hydrology,CAS, Wuhan 430072,China);Effects of Endocrine Disrupting Chemicals on Animals and Mechanisms of Action[J];RESEARCH OF ENVIRONMENTAL SCIENCES;2000-06
3 Dai Shugui,Zhang Dongmei,Zhang Renjiang,Zhang Lin,Jin Sansan(College of Environmental Science & Engineering of Nankai University,Tianjin 300071,China E mail:sgdai@publicl.tpt.tj.cn);Isolation of Phthalate Esters in Aquatic Samples by C_(18) Bonded Phase Extraction Column[J];CHINESE JOURNAL OF ENVIROMENTAL SCIENCE;2000-02
4 Wu Pinggu,Han Guangen,Wang Huihua,et al.Zhejiang Province Sanitation and Anti epidemic Station,Hangzhou 310009;An Investigation on Phthalates in Drinking Water[J];JOURNAL OF ENVIRONMENT AND HEALTH;1999-06
5 HAN Guan gen,WU Ping gu,WANG Hui hua,et al Zhejiang Provincial Center for Disease Prevention and Control,Hangzhou 310009;Pollution of Municipal Water Supply System by Phthalates and Evaluation on Purification Effects of Current Water Treatment Process[J];Journal of Environment and Health;2001-03
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved