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《China Powder Science and Technology》 2006-04
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Preparation of ZrO_2(3Y) Nanoceramics Under Two-stage Non-pressurized Sintering

XU Hai-jun~1 LI Jia~2 SHI Rui-xia~2 (1.Inner Mongolia Chemical Engineering Professional College,Huhhot 010010; 2.School of Material Science and Engineering,Jinan University,Jinan 250022,China)  
The compatible controlling for grain growth and densifica- tion of ZrO_2(3Y) nanoceramics under two-stage non-pressurized sinter- ing was investigated.The ZrO_2(3Y) nano-particles with the grain size of 30 nm was compacted by applying cold isostatic press of 430 MPa.The green pellets with the relative density of 49%was heated to 1250℃to obtain 94% relative density,then cooled down to 1 050℃and holding for 20 h until it was fully dense.The final grain size was 100 nm.The results showed that the sticking point of non-pressurized sintering was to find out the compatible area wherein grain growth was suppressed and densification maintain by exploiting the difference in kinetics be- tween grain-boundary diffusion and grain-boundary migration.
【Fund】: 国家自然科学基金,编号:50572034。
【CateGory Index】: TB383.1
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