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《Chinese Journal of Analytieal Chemistry》 1998-08
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Synthesis of Bonded Stationary Phase of 5, 10, 15,20- Tetrakis(4-hydroxyphenyl)porphine-silica and Its Application to the Nucleotides Analysis

Huang Chaoyang, Shi Xuejun, Liang Shuwen, Yu Shilin (Department of Applied Chemistry, Beijing University of Chemical Technology, Beijing 100029) Sheng Ziliang (Xianning Education Institute of Hubei Province, Xianning 437100)  
5,10,15,20-Tetrakis (4-hydroxyphenyl) porphine (THPP ) had been synthesized and used as a stationary phase ligand. A wide-pore(30 nm), microspheric silica(8μm) as the matrix activated by γ aminopropyltriethoxysilane, then reacted with spacer arm-epichlorohydrin, and bonded with the THPP li- gand to produce a new stationary phase of charge-transfer type-THPP-silica. When phosphate buffer(pH =7. 0) was used as the mobile phase, the separation of nucleosides and nucleotides was achieved by the detection of ultraviolet detector (254 nm).
【CateGory Index】: O658
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