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《Chinese Journal of Analytieal Chemistry》 1998-08
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Study on the Chemiluminescence Reaction between Lucigenin and Iron (Ⅱ)by Flow -Injection Analysis With Micelle Sensitization

Zhu Zhijia (Experimental Center, Hebei Normal University, Shijiazhuang 050016) L■ Jiuru (Department of Chemistry, Shanxi Normal University, Xi'an 710062)  
A new flow-injection chemiluminescence method for the determination of iron is described. It is based upon the chemiluminescence reaction of iron (Ⅱ)-lucigenin system with Jones reductor. The chemiluminescence signal-to-noise ration can be improved apparently by the addition of cetyltrimethyl- ammonium bromide and emulsor OP. The present method has a wide linear of 1×10-11~1×10-5 g/mL for Fe(Ⅱ). The detection limit is 2 × 10-12 g/mL. The relative standard deviation is 2.0% (1× 10-8 g/mL Fe, n = 11). The method has been applied to the determination of iron in hair samples with satisfactory results. The mechanism of this reaction is also investigated in detail.
【CateGory Index】: O657.3
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