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《Chinese Journal of Analytical Chemistry》 2003-04
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Rapid Analysis of Eleutheroside by Electrospray Tandem Mass Spectrometry

Guo Mingquan, Song Fengrui, Liu Zhiqiang ,Liu Shuying * (Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022)  
Eleutheroside B (syringin) and Eleutheroside E (syringaresinol diglycoside) which were considered to be effective constituents from a canthopanax senticosus Harms (AS) were determined in the extracts of AS by electrospray tandem mass spectrometric (ESI-MS n) methods after micro-column chromatographic separation. Their molecule masses were detected and ESI-MS n data were obtained, and fragmentation mechanisms were proposed. Their characteristic mass spectra can be used as fingerprint for the identification of Eleutheroside B and E from AS. This method is simple, rapid and highly sensitive and reproducible, and plays important role in the quality control of AS drugs.
【Fund】: 吉林省科技厅重点发展项目 (No .19990 310 2 )资助课题
【CateGory Index】: O657.63
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