Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chinese Journal of Analytical Chemistry》 2003-04
Add to Favorite Get Latest Update

Rapid Analysis of Eleutheroside by Electrospray Tandem Mass Spectrometry

Guo Mingquan, Song Fengrui, Liu Zhiqiang ,Liu Shuying * (Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022)  
Eleutheroside B (syringin) and Eleutheroside E (syringaresinol diglycoside) which were considered to be effective constituents from a canthopanax senticosus Harms (AS) were determined in the extracts of AS by electrospray tandem mass spectrometric (ESI-MS n) methods after micro-column chromatographic separation. Their molecule masses were detected and ESI-MS n data were obtained, and fragmentation mechanisms were proposed. Their characteristic mass spectra can be used as fingerprint for the identification of Eleutheroside B and E from AS. This method is simple, rapid and highly sensitive and reproducible, and plays important role in the quality control of AS drugs.
【Fund】: 吉林省科技厅重点发展项目 (No .19990 310 2 )资助课题
【CateGory Index】: O657.63
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【References】
Chinese Journal Full-text Database 4 Hits
1 CHAI Yi feng ,WU Yu tian andLI Xiang(Department of Pharmaceutical Analysis ,College of Pharmacy ,Second Military edical University ,Guohe Road 32 5 , Shanghai 2 0 0 4 33);Pharmaceutical Analysis (Ⅱ)[J];Analytical Laboratory;2004-07
2 YUAN Ye-rong1,LI Qiang2(1.Dalian Friendship Hospital,Dalian 116001,Liaoning,China;2.Shengyang Funing Pharmaceutical Factory,Shenyang 110042,Liaoning,China);Study on Isolation Syringin and Determination the Concentration of Syringin in Acanthopanax Senticosus Harms[J];Liaoning Journal of Traditional Chinese Medicine;2007-06
3 YU Hai-yan1,2,WU Xiang-yu1,2,ZHANG Li-min1,TANG Hui-ru1 [1.State Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Center of Magnetic Resonance (Wuhan Institute of Physics and Mathematics,Chinese Academy of Sciences),Wuhan 430071,China; 2.Graduate School of the Chinese Academy of Sciences,Beijing 100049,China];Analysis of Phytomedicines[J];Chinese Journal of Magnetic Resonance;2012-01
4 SUN Xiu-ting;WANG Shun-xian;JIANG Jian-lan;Tianjin Key Laboratory of Biological and Pharmaceutical Engineering,Department of Pharmaceutical Engineering,School of Chemical Engineering and Technology,Tianjin University;Tianjin Shijitianlong Pharmaceutical Co. Ltd.;;Research on Identification and Determination of Multiple Components in Longjiatongluo Capsule[J];Journal of Instrumental Analysis;2015-01
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 TIAN Shi-lin et al (Huanghuai University Agriculture and Forestry Institute,Zhumadian,Henna 463000);Determination of the Content of Aucubin in Wild Plantago asiaca Grown in Southern Henan[J];Journal of Anhui Agricultural Sciences;2006-19
2 MA Rui,XU Huan,YANG Li-li,CHENG Liang,TANG Yun-guo,YE Yun(Grade 2001,Faculty of Medicine,Bengbu Medical College,Bengbu 233030,China);Protective effect of acanthopanax senticosus injection on the acute myocardial anoxia in mice[J];Journal of Bengbu Medical College;2006-01
3 Su Mingjun1,Zhang Lihua2 (1.Affiliated Hospital of Chifeng College;2.Chifeng Tianqi Pharmaceutical Co.Ltd,Inner Mongolia Chifeng 024000);Determination of schizandrin in Shenmai soft capsules by HPLC[J];Journal of North Pharmacy;2010-01
4 ZHAO Yin-chun,LIAO Ming-an,WANG Mi-li,LIU Xu(College of Forestry and Horticulture,Sichuan Agricultural University,Yaan,Sichuan 625014,China);A Study on Quality Changes During Fruit Development of Chilii Pepper[J];Northern Horticulture;2008-07
5 Ren Difeng;Wang Jianzhong;Wang Xiaonan. School of Biological Science and Biot echnology,Beijing For. Univ. ,100083,P. R. China.;Deteriorative kinetics of Rehmannia glutinosa and Ophiopogon japonic us during drying[J];Journal of Beijing Forestry University;2004-01
6 YOU Yan,CHEN Kai,LI Huan-rong*,HOU Yuan-yuan(College of Food Science,Xinjiang Agricultural University,Urumqi 830052,China);Optimization of Extraction of cAMP Response Surface Methology[J];Storage & Process;2011-02
7 ZHAO Ren-bang,CUI Tong,GUO Xiu-min,GE Wei, ZHANG Dong,LIU Shu-chen (Deqartment of Food,Agricultural University of Hebei,Baoding 071001,China);Determination of capsiciu by high performance liquid chromatography[J];Journal of Agricultural University of Hebei;2002-04
8 Cheng Guangyou,Tang Xiaojie(College of Forestry,Beihua University,Jilin 132013,P.R.China);Gou Yufan(Popularization Center of Agricultural Technique of Da'an City,Jilin Province);Hu Baice(Institute of Forest Inventory and Planning,Jilin Province);Variation of Matrine Content in Intraspecies of Sophora flavescens[J];Journal of Northeast Forestry University;2010-01
9 LIU Jie-shu ( Medical College, Hubei Institute for Nationalities, Enshi 445000, China);Potency and Use Differences between Peucedanum Terebinthaceum and Saposhnikouia Divaricata[J];Journal of Hubei Institute For Nationalities Medical Edition;2003-02
10 Bao Guorong. Chen Dan. Luo Zhiyi (Department of pharmacy, Fujian College of Traditional Chinese Medicine, Fuzhou Fujian, 350003);Determination of emodin in kangxin oral solution by HPLC[J];Fujian Analysis&Testirg;2004-01
China Proceedings of conference Full-text Database 2 Hits
1 ;HPLC法测定精制海马追风膏中士地宁的含量[A];[C];2006
2 Jian-Hui Zhang,Yu-Tang Wang,Chang-li Bao*,Wei-Wei Kong,Fei Li Collage of Chemistry, Jilin University, Changchun 130012;Separation and Enrichment of the Active Constituents in Radix Et Rhizoma Rhei by Solvent Sublation[A];[C];2008
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 FENG Ying et al (Food College,Shenyang Agricultural University,Shenyang,Liaoning 110161);Determination and Extraction of Flavonoids in Fruit of Acanthopanax Sessiliflorus Seem[J];Journal of Anhui Agricultural Sciences;2006-12
2 WANG Juan,SHOU Sen-yan(Department of Horticulture, Zhejiang University, Hangzhou 310029);Effects of High Temperature Stress on Chlorophy11 and Autioxidant Systems in Lettuce Seedlings[J];Northern Horticulture;2007-02
3 MENG Xiang-cai,YU Dong-mei,SUN Hui,WANG Xi-jun (Heilongjiang university of Chinese medicine,Harbin,Heilongjiang 150040);The Effect of Different Environment on Physiological,Biochemical and Photosynthesis of Acanthopanax senticosus[J];Northern Horticulture;2010-12
4 Wen Jing\ \ Jin Zonglian (College of Applied Sciences and Humanities of BUU,Beijing\ 100083);Quantitative Analysis of Adenosine Content in Rat Brain[J];JOURNAL OF BEIJING UNION UNIVERSITY;1997-01
5 CAO Xia 1,GAO Yu fei *,LI Hong 1,YANG Hong 1,YANG Shi jie 1,DU Xue rong 2 (1 Dept.of Pharmacology,School of Basic Medical Sciences,Jilin University,Changchun 130021 China; 2\ Department of Chinese Traditional Medicine,China Japan Union Hospit;Comparative study of effects of Ginsenosides,Panaquilons and Eleutherosides on isolated working heart[J];Journal of Norman Bethune University of Medical Science;2001-03
6 ZHANG Man ying,AN Ji hong,LI Chang hui (Dept.of Respiration,The Second Hospita,Jilin University,Changchun 130021 China);Study on apoptosis of Spc-A_1 cell induced by acanthophopanax senticosus[J];Journal of Norman Bethune University of Medical Science;2002-01
7 JIANG Hong yu 1,SUI Da yuan 1 ,YU Xiao feng 1,QU Shao chun 1,XU Hua li 1,WANG Zhi cai 2,CHEN Yan ping 2 (1.Department of Pharmacology, School of Pharmacy, Jilin University,Changchun 130021, China; 2.Department of Nature Medical Chemistry, School of Chemistry, Jilin University, Changchun 130021, China);Effects of Acanthopanax senticosus saponins(ASS) on hemorrheology and platelet function in experimental cerebral ischemia rats[J];Journal of Jilin University of (Medicine Edition);2004-03
8 LI Yang,QU Shao-chun,YU Xiao-feng,XU Hua-li,SUI Da-yuan~*(Department of Pharmacology,School of Pharmacy,Jilin University,Changchun 130021,China);Effect of Acanthopanax senticosus saponins on organ blood flow in anesthetized dogs[J];Journal of Jilin University(Medicine Edition);2006-06
9 Zhan Shu,Liu Wei,Shao Chunjie et al(Dept.of physiology,Central Laboratory of Physioloy,Dept.of organic chemistry);Influence of acanthopanax senticosides B(Sb)on the action potential of cultured myocardial cells in rats[J];JOURNAL OF NORMAN BETHUNE UNIVERSITY OF MEDICAL SCIENCE;1995-01
10 Zhan Shu,Sun Ckenwen,Zhong Guogan,et al(Dept.of Physiol,Central Lab.of Phyxiol);Influence of Ass on blood flow dynamics of isol ated working heart[J];JOURNAL OF NORMAN BETHUNE UNIVERSITY OF MEDICAL SCIENCE;1995-04
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 Fu Ruo-nong(Department of Chemistry Beijing Institute of Technoligy, Beijing 100081);Advances on gas chromatography in China in recent two years(Ⅱ)[J];Analytical Laboratory;2005-05
2 XIA Guo-Chao TAO Hui-Lin(Dept. of Material and Chemical Engi.,Guilin Institute of Tech.,Guilin,Guangxi 541004,P.R.China);Spectrophotometric Studies on Three-Fluorescence and Resonance Scattering of Rhodamine 6G[J];Chinese Journal of Spectroscopy Laboratory;2008-05
3 LIU Ke-ling Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100080, China;Review of Atomic Spectroscopy[J];Spectroscopy and Spectral Analysis;2005-01
4 DENG Wu-yuan;ZOU Jia-li;HE Qi-yi;ZHAO Yin;DENG Ke-xuan;ZHANG Jin-chun;YANG Xian;YU Xiao-dong;LUO Tong;Institute of Biology,Yibin University;School of Life Science,Chongqing Normal University,Chongqing Key Laboratory of Animal Biology,Chongqing Engineering Research Center of Bioactive Substance;;Methods and Processes for Extracting Polyphnols from the Flowers of Camellia japonica[J];Journal of Chongqing Normal University(Natural Science);2013-05
5 ZHANG Xiu-li,WANG Xin-ying,SHI Lan-xiang(College of Materials Science and Engineering,China Geology University,Beijing 100083,China);Determination of 7-amido acetoxy eicosanoic acid by ultraviolet spectrophotometric method[J];Chemical Engineer;2006-07
6 GAO Leng,HAN Xue,LI Ning(School of Chemistry and Life Science,Changchun University of Technology,Changchun 130012,China);Study on the extraction process for syringin by technology of ultrasonic[J];Chemical Engineer;2011-01
7 ZHAO Yan-jing WANG Chen (Jiangsu Key Laboratory of Marine Biotechnology,Huaihai Institute of Technology,Lianyungang 222005);Preliminary studies on extraction and anticancer activity of a protein from Sinonovacula constrzcta[J];Progress in Fishery Sciences;2011-06
8 ;The antitumor effects of acanthopanax senticosus components[J];Journal of Jilin Medical College;2014-05
9 LI Juan;WANG Juan;ZHU Ya;LU Bin-bin;WANG Ke-ming;WANG Zhao-xia;WANG Ji-rong;Department of Oncology, the Second Affiliated Hospital of Nanjing Medical University;;Clinical research on Aidi injection combined with chemotherapy in the treatment of advanced NSCLC[J];Hainan Medical Journal;2014-23
10 HUANG Tao1,LI Xu-hui2,ZOU Chun-ping1,LI Xiu-cheng1,FENG Dian-peng1 1.Department of Orthopedics,First Affiliated Hospital of China Medical University,Shenyang 110001, P.R.China 2.School of Life Sciences,Tsinghua University,Beijing 100084,P.R.China;Killing effect of osteosarcoma cells induced by combination of AiDi and doxorubicin[J];Chinese Journal of Cancer Prevention and Treatment;2012-09
China Proceedings of conference Full-text Database 1 Hits
1 ZHANG Bei-yue;WEI Yong-heng;SHI Jin-li;Beijing University of Chinese Medicine;;Research Progress of the Chemical Constituents and Pharmacological Effects of Leaves of Acanthopanax senticosus(Rupr.et Maxim.) Harms.[A];[C];2015
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved