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《Chinese Journal of Analytical Chemistry》 2010-04
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Preparation and Properties of Diethylstilbestrol Molecular Imprinted Polymers Sensor

LIU Ying ,GUAN Liang-Hui,HUANG Xin,SONG Qi-Jun(School of Chemical and Material Engineering,Jiangnan University,Wuxi 214122)  
An electrochemical sensor based on electropolymerized molecularly imprinted polymers(MIPs)for diethylstilbestrol(DES)detection is reported.The sensor was prepared by electropolymerizing o-phenylenediamine(OPD)on a glassy carbon electrode in the presence of template diethylstilbestrol.Template can be quickly removed by 50%(volume fraction)ethanol-water solution.The analytical performance of the molecularly imprinted polymer was studied and indirect analytical method based on the medium of potassium ferricyanide was established.A linear relationship between the concentration of DES and relative peak current change of potassium ferricyanide was obtained with a range from 1.0×10 -7 to 5.1×10 -6 mol/L.The result shows that this sensor provides an efficient way for eliminating interferences from compounds with similar structures to that of DES.
【Fund】: 江南大学青年基金(No.20070344)资助项目
【CateGory Index】: TP212.2;O657.1
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