Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chinese Journal of Analytical Chemistry》 2011-06
Add to Favorite Get Latest Update

Solid Phase Extraction of Ursolic Acid Using Imprinted Polymer Modified Multi-walled Carbon Nanotubes

LIU Xi1,ZHANG Zhao-Hui*1,2,ZHANG Hua-Bin1,HU Yu-Fang1,YANG Xiao1,NIE Li-Hua2 1(College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000) 2(State Key Laboratory of Chemo/Biosensing and Chemometrics,Hunan University,Changsha 410082)  
A novel surface imprinting material based on multi-wall carbon nanotubes(MWNT/MIPs) modified with polyethylene glycol was successfully synthesized with a precipitation polymerization method by using ursolic acid(UA) as template,methacrylic acid(MAA) as functional monomer,and ethylene glycol dimethacrylate (EGDMA) as cross-linker.The MWNT/MIP was characterized by IR and scanning electron microscopy (SEM).The results showed that a stable,uniform imprinted materials layer was grafted on the surface of MWNT.The adsorption capacity of UA on MWNT/MIPs was measured by high performance liquid chromatography.A maximum apparent adsorption capacity of 100.1 μmol/g for the imprinted polymers toward UA was obtained.As solid phase extraction materials,the imprinted polymers extracted UA from actinidia chinensis planch successfully with the concentration enrichment factor of 5.35.
【Fund】: 国家自然科学基金(No.21005030);; 湖南省教育厅重点项目(No.10A099);; 湖南省科技计划项目基金(No.2009FJ3009);; 湖南省大学生创新基金(No.JSU-CX-2010-46)资助
【CateGory Index】: TQ461
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 6 Hits
1 ZHANG Zhao-Hui1,2,ZHANG Hua-Bin1,WU Yu-Fang1,LIU Li1,LI Hui1,2,YAO Shou-Zhuo2(1.College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,China;2.State Key Laboratory of Chemo/Biosensing and Chemometrics,Hunan University,Changsha 410082,China);Proparation and Characterization of Stereoselective L-Histidine Imprinted Microspheres[J];Chemical Journal of Chinese Universities;2008-10
2 LIU Xian-Jun1,2,ZHANG Jing2,SHAO Bing1,2,YIN Jie1,3 1(Central Laboratory,Beijing Center for Disease Control & Prevention,Beijing 100013) 2(School of Public Health and Family Medicine,Capital Medical University,Beijing 100058) 3(School of Public Health,Peking University,Beijing 100191);Determination of Tamoxifen and Letrozole in Sewage by Solid Phase Extraction and Ultra Performance Liquid Chromatography/Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2010-02
3 WANG Jiang-Tao1,SONG Xing-Liang1,2 1(Key Laboratory of Marine Chemistry Theory and Technology,Ministry of Education,Ocean University of China,Qingdao 266100) 2(Linyi Normal University,Linyi 276005);Synthesis,Evaluation and Adsorption Behavior of Naphthalene Analog-Imprinted Polymer by Immobilized Template on Modified Silica Gel in Seawater[J];Chinese Journal of Analytical Chemistry;2010-08
4 LIU, Qiu-Yea LI, Wen-Youa HE, Xi-Wen*,a CHEN, Lang-Xinga ZHANG, Yu-Kui*,a,b (a Department of Chemistry, Nankai University, Tianjin 300071) (b Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116011);Study of Recognition Property of Molecularly Imprinted Bovine Hemoglobin on Surface-modified Silica Gel[J];Acta Chimica Sinica;2008-01
5 SI Fu-ting,LI Jing-jing,ZENG Chao,SI Fang-bo,ZHOU Xiao-li(College of Chemical & Food Engineering,Zhongzhou University,Zhengzhou 450044,China);Research Progress of Antitumor Activity and Mechanism of Ursolic Acid[J];Chemistry & Bioengineering;2010-01
6 LIN Fuhua,HUANG Xiaojia,YUAN Dongxing,LIU Baomin(State Key Laboratory of Marine Environmental Science,Environmental Science Research Center,Xiamen University,Xiamen 361005,China);Determination of bisphenol A in environmental water samples by stir bar sorptive extraction based on molecularly imprinted polymer[J];Chinese Journal of Chromatography;2010-05
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 ZHANG Hua-Bin 1,ZHANG Zhao-Hui 1,2,HU Yu-Fang 1,YANG Xiao 1,NIE Li-Hua2(1.College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,China;;Preparation and Adsorption Properties of p-Nitrophenol Imprinted Materials Based on Multi-walled Carbon Nanotubes Surface[J];Chemical Journal of Chinese Universities;2010-11
2 ZHANG Cheng-li1, ZHOU Yan-mei1, LEI Jian-du2, MA Tong-sen1, MA Guang-hui2, SU Zhi-guo2 (1. College of Chemistry and Chemical Engineering, Henan University, Kaifeng, Henan 475004, China; 2. State Key Lab. Biochemical Engineering, Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China);Synthesis of Molecularly Imprinted Polymer for Rifampicin and Its Adsorption[J];The Chinese Journal of Process Engineering;2009-03
3 YANG Yun,LIAN Hui-ting,LIU Bin,SUN Xiang-ying(College of Material Science and Engineering,Huaqiao University,Quanzhou 362021,China);Preparation and Properties of Trichlorfon Molecularly Imprinted Polymers[J];Journal of Huaqiao University(Natural Science);2009-03
4 Tang, Kaijiea,b,c Gu, Xiaohonga Zhu, Songa Tang, Jian*,a Wang, Haijund (a State Key Laboratory of Food Science & Technology, Jiangnan University, Wuxi 214122) (b College of Food Science & Engineering, Jiangxi Agriculture University, Nanchang 330045) (c School of Food Science & Technology, Jiangnan University, Wuxi 214122) (d School of Chemical & Material Engineering, Jiangnan University, Wuxi 214122);Spectrum Analysis and Adsorption Characteristics of Bensulfuron-methyl Molecularly Imprinted Polymers[J];Acta Chimica Sinica;2009-07
5 ZHANG ZhaoHui1,2,ZHANG HuaBin1,HU YuFang1 & YAO ShouZhuo1 1. College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,China; 2. State Key Laboratory of Chemo/Biosensing and Chemometrics,Hunan University,Changsha 410082,China;Preparation and characterization of stereoselective L-histidine imprinted polymer on multiwalled carbon nanotubes[J];Science in China(Series B:Chemistry);2009-06
6 Zhang,Zhaohui,a,b Hu,Yufanga Zhang,Huabina Li,Huia,b Yao,Shouzhuob (aCollege of Chemistry and Chemical Engineering,Jishou University,Jishou 416000) ( b State Key Laboratory of Chemo/Biosensing and Chemometrics,Hunan University,Changsha 410082);Preparation and Evaluation of Caffeine Molecularly Imprinted Composite Membrane[J];Acta Chimica Sinica;2009-18
7 Wen,Qianga,b Zhang,Mingleib Zhang,Zhaohui ,a,b,c Zeng,Yunb Nie,Lihuac (a Hunan Province Key Laboratory of Forest Product and Chemical Engineering,Jishou 416000)(b College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000)(c State Key Laboratory of Chemo/Biosensing & Chemometrics,Hunan University,Changsha 410082);Microwave-assisted Heating for Rapid Preparation and On-line Enrichment Application of Core-shell Uridine Imprinted Polymer[J];Acta Chimica Sinica;2011-02
8 Zhu,Guifena Gao,Yanbua Gao,Xiaa,b Fan,Jing*,a(a School of Chemistry and Environmental Science,Key Laboratory for Yellow River and Huai River Water Environment and Pollution Control of Ministry of Education,Henan Key Laboratory for Environmental Pollution Control,Henan Normal University,Xinxiang 453007)(b School of Public Health,Xinxiang Medical University,Xinxiang 453003);Preparation and Separation Properties of Gatifloxacin Molecularly Imprinted Polymer Microsphere[J];Acta Chimica Sinica;2011-08
9 BI Liang-wu,LI Da-wei,ZHAO Zhen-dong,LI Dong-mei (Institute of Chemical Industry of Forest Products,CAF;National Engineering Lab.for Biomass Chemical Utilization;Key and Open Lab.on Forest Chemical Engineering,SFA;Key Lab.of Biomass Energy and Material,Jiangsu Province,Nanjing 210042,China);Review on Development and Comprehensive Utilization of Rosemary Resources[J];Biomass Chemical Engineering;2011-03
10 XIONG Zhen-hu,YU Wan-lu(Department of Environmental and Municipal Engineering,TIUC,Tianjin 300384,China);Recent Developments in Molecularly Imprinted Polymers for Selective Recognition of Deleterious Organic Pollutants at Trace Concentration in Aqueous Media[J];Journal of Tianjin Institute of Urban Construction;2009-03
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 WANG Jie Jun 1, WANG Bing 1, GUO Jing 1, GAO Yong 1, XU Qing 1, CHEN Wan Sheng 2 (1. Department of Oncology, Changzheng Hospital, Second Military Medical University, Shanghai 200003, China; 2. Department of Pharmacognosy, College of Pharmacy);Inhibitory effect of ursolic acid on angiogenesis in vitro[J];Academic Journal of Second Military Medical University;2000-11
2 L Gang1,2,WANG Li-bing2,LIU Jun2 and LI Shu-fen1(1.Tianjin Entry Exit Inspection and Quarantine Bureau,Tianjin 300042;2.Institute of Chemical and Engineering Tianjin University,Tianjin 300072);Determination of phenolic environmental estrogens in packaging materials by solid phase micro-extraction-gas chromatography coupled mass spectrometry(SPME-GCMS)[J];Chinese Journal of Analysis Laboratory;2008-09
3 ZHANG Shu-Qiong 1,YANG Huang-Hao 2,ZHUANG Zhi-Xia 1,2,* ,WANG Xiao-Ru 1,2 [WT5”BX](1. The Key Laboratory of Analytical Sciences of MOE,Department of Chemistry, Xiamen University,Xiamen 361005,China; 2. Material Transport & Transformation in Environmental & Life Processes Lab, The First Institute of Oceanography,SOA,Qingdao 266061,China) [WT5HZ];Preparation of Molecular Imprinting Sol-gel Nanotubes Membrane and Its Application to Biochemical Separations[J];Chemical Research In Chinese Universities;2004-06
4 LI Yong+{1,2}, YANG Huang-Hao+{1*}, ZHUANG Zhi-Xia+1, WANG Xiao-Ru+1 (1. The First Institute of Oceanography, SOA, Qingdao 266061, China; 2. Wenzhou Medical College, Wenzhou 325000, China);Surface Molecularly Imprinted Polymer Nanowires Used for Protein Recognition[J];Chemical Research In Chinese Universities;2005-09
5 LI Li~1,HU Shu-Guo~1,HE Xi-Wen~(1*),LI Wen-You~1,CHEN Lang-Xing~1,ZHANG Yu-Kui~(1,2*)(1.College of Chemistry,Nankai University,Tianjin 300071,China;2.Dalian Institute of Chemical Physics,Chinese Academy of Sciences,Dalian 116023,China);Solid-phase Extraction of Active Component of Chinese Traditional Medicine Fisetin by Using Molecularly Imprinted Polymers[J];Chemical Journal of Chinese Universities;2006-04
6 Fan Mingwen, Wang Qian, Bian Zhuan, et al Department of Endodontics,School of Stomatology, Wuhan University, Wuhan 430079, China;Effect of Ursolic Acid on the Human Tongue Squamous Carcinoma Cell Line TSCCa and Possible Mechanism[J];Journal of Hubei Medical University;2004-01
7 LUO Ting-liang , ZHANG Jing-wei , CAO Wen-hao , LUO Na , LIU Guo-ji(Institute of Chemical Engineering , Zhengzhou University , Zhengzhou450002 , China);Research Progress on Extraction Process of Ursolic Acid from Fructus Corni[J];Henan Chemical Industry;2005-02
8 Song Xijin, Gong Wei, Wang Jie# (Institute of Pharmaceutical Engineering, #Department of Chemistry, Zhejiang University, Hangzhou 310027);Proteins Molecular Imprinted Technique[J];Chemistry;2005-07
9 ZHANG Qiu-ping, XIE Luo-kun, DENG Tao, et al. (Department of lmmunology, Medical School of Wuhan University, Wuhan 430071, China);Ursolic acid enhances apoptosis in K562 cells[J];Basic Medical Sciences and Clinics;2004-04
10 WANG Bing,WANG Jie jun,XU Jun,et al.Department of Radiation Oncology,Shanghai Sixth People's Hospital,Shanghai 200233,China;Inhibitory Effects of Ursolic Acid on Angiogenesis in Vitro[J];Journal of Qilu Oncology;2001-04
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved