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《Journal of Analytical Science》 1993-03
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Study on Separation for Mix Of Phenols and Alkylation Products Of Pyrazine Using High Performance Liquid Chromatograpy with Simplex

Min shungeng Deng bo Chen pcirong (Department of Chemistry,Tsinghua Uniuersity, Beijing,100084)  
The separation conditions for mix containing phenol, o-methylphenol、p-diphenol、o-diphenol、o-nitrophenol and α-naphthol as well as alkylation products of pyrazine were investigated and the effects of various parameters on separation discussed. A comprehensive evaluation criterion for HPLC optimization separation was proposed and the methods for separation mix of phenols and alkylation of pyrazine were established. This method has been applied to the separation of the complex system containing six phenols and alkylation products of pyrazine. The satisfactory results of separation were obtained using the optimal conditions obtained by MSM optimization.
【Fund】： 国家自然科学基金
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【References】
Chinese Journal Full-text Database 3 Hits
1 Mo Hua,Deng Bo, (Department of Chemistry, Tsinghua University, Beijing 100084);Study on Optimizing of Separation Conditions for Mixtures of Phenols With High-performance Liquid Chromatography by Using Artificial Neural Network[J];Chinese Journal of Analytieal Chemistry;1995-07
2 Deng Bo (Department of Chemistry, Tsinghua University, Beijing, 100084, China);Studies on Optimization Method of Experiment[J];JOURNAL OF ANALYTICAL SCIENCE;1996-02
3 Gong Xiaoyi;Deng Bo;Luo Guoan(Department of Chemistry,Tsinghua Unviersity Beijing 100084);A GENERATOR FOR FEEDFORWARD ARTIFICIAL NEURAL NETWORK[J];COMPUTERS AND APPLIED CHEMISTRY;1996-04
【Citations】
Chinese Journal Full-text Database 1 Hits
1 Deng Bo, Chen Pejrong. Cai Xiaojia (Department of Chemistry, Tainghua University, Beijing);Simplex Optimization of HPLC to Separate and Determine Vitamin E Isomers[J];Chemical Research In Chinese Universities;1988-04
【Co-citations】
Chinese Journal Full-text Database 4 Hits
1 Xu Minliang (Central-South Institute of Mining and Metallurgy);Simplex Optimization Method in Analytical Chemistry[J];Chinese Journal of Analytical Chemistry;1984-02
2 Deng Bo (Department of Chemistry, Tsinghua University, Beijing, 100084, China);Studies on Optimization Method of Experiment[J];JOURNAL OF ANALYTICAL SCIENCE;1996-02
3 Deng Bo (Department of Chemistry, Tsinghua University, Beijing 100084;Analytical Chemometrics[J];Chinese Journal of Analysis Laboratory;1991-04
4 Mao Dongsen(Shanghai Research Institute of Petrochemical Technology,Shanghai,201208);Uniform Design and its Applications in Chemical Industry[J];Chemical Industry and Engineering Progress;1997-05
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 Nie Hengrui,Guo Shucai, Zhao Shuchang Lin Qi and Cui Zhidong;Research on Rapid Pyrolysis of Brown Coal and Oil Shale[J];;1982-04
2 Zhao Shuchang, Liu Guixiang, Dong Zhenwen and Nie Hengri Coal Chemical Engineering Research Group of D. I. T.;The Influence of Temperature on Coal Tar Composition of Shulan Brown Coal by Rapid Pyrolysis[J];;1982-04
3 Cai Yudong , Wu Wei, Gan Junren, Yao Linsheng (Shanghai Institute of Metallurgy, Chinese Academy of Sciences, Shanghai 200050);Determination of Potential Titration End-point by Neural Network[J];Chinese Journal of Analytical Chemistry;1993-04
4 Liu Qiang (Department of Applied Chemistry, Taiyuan University of Technology, Taiyuan 030024)Deng Bo (Department of Chemistry, Tsinghua University, Beijing 100084);Atomization Mechanism of the Elements on the Graphite Probe Surface in the Graphite Furnace Ⅶ. The Atomization Mechanism of Germanous Fluoride and Sodium Germanate[J];Chinese Journal of Analytical Chemistry;1993-11
5 Deng Bo, Min Shungeng (Department of Chemistry, Tsinghua University. Beijing 100084);Comparison on Optimization Properties of Some Simplexes[J];Chinese Journal of Analytieal Chemistry;1994-03
6 Mo Hua,Deng Bo, (Department of Chemistry, Tsinghua University, Beijing 100084);Study on Optimizing of Separation Conditions for Mixtures of Phenols With High-performance Liquid Chromatography by Using Artificial Neural Network[J];Chinese Journal of Analytieal Chemistry;1995-07
7 Deng Bo and Wang Xiaoqin (Department of chemistry, Tsinyhua Unversity);Study on Determination Parameters of Platinum by GFAAS Using Orthogonal Polynomial Regression Design[J];Chinese Journal of Analysis Laboratory;1986-04
8 Deng Bo (Department of Chemistry, Tsinghua University, Beijing 100084);Advances in Analytical Chemometrics[J];Analytical Laboratory;1993-04
9 BaiWenmin;DengBo andCaiXiaojia (Department of Chemistry,Tsinghua Universi-ty,Beijing 100084);Strdy on the CGC/AAS and Analysis of the Speciesof Trace Selenium in Garlic Oil[J];ANALYTICAL LABORATORY;1994-01
10 Deng Bo, Chen Pejrong. Cai Xiaojia (Department of Chemistry, Tainghua University, Beijing);Simplex Optimization of HPLC to Separate and Determine Vitamin E Isomers[J];Chemical Research In Chinese Universities;1988-04
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Chinese Journal Full-text Database 10 Hits
1 Geng Xinqing (AISC Iron and Steel University);Artificial Nervous Network Development in Stoichiometry[J];;2001-03
2 LIU Li-hua et al(Eastern Liaoning University,Dandong,Liaoning 118003);Evaluation of Experiment Design before Implementation[J];Journal of Anhui Agricultural Sciences;2006-06
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7 Deng Bo (Department of Chemistry, Tsinghua University, Beijing, 100084);A retrospect of development of atomic absorption spectrophotometric techniques in China in the past 30 years .[J];Analytical Instrumentation;2002-01
8 Wang Dan,Fang Liguo(Chemistry & Energy College,South China University of Technology,Guangzhou 510640,China);Research Development on the Application of Neural Network in Chemical Industry[J];Guangdong Chemical Industry;2007-10
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10 YE Long\|Jun (Lipu Teachers School, Lipu,Guangxi 546600, P.R.China) MENG Dan\|Jun\ LIN Hui\|Song (Guangxi Vocational\|Technical College, Nanning 530227, P.R.China);Studies on a High Sensitivity Reaction of Vanadium (Ⅴ) with Diantipyryl-(o-Ethoxy)-Phenylmethane (DAoEM) by Orthogonal Design[J];Chinese Journal of Spectroscopy Laboratory;2002-03
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