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《Journal of Analytical Science》 1993-03
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Separation and determination of V(Ⅴ). Co(Ⅱ). Ni(Ⅱ).Cu(Ⅱ)and Cr(Ⅵ) as their complexes with 4-(6-methyl-2-benzothiazolyazo) resorcinol by reversed-phase HPLC

Miao Yuxia,Wang Hong, Zhang Huashan and Cheng Jieke (Department of Chemistry, Wuhan University, Wuhan 430072)  
The RP-HPLC separation and determination of V(Ⅴ), Co(Ⅱ), Ni (Ⅱ),Cu (Ⅱ) and Cr (Ⅵ) using MBTAR as precolumn derivative reagent was reported in this paper. Methanol-water (75/25,v/v) containing 15mmol/L TBA Br, 10mmol/L pH=6.0 HAc-NaAc buffer solution was used as the mobile phase. The five complexes can be separated completely within 16 minutes. When S/N=3, the detection limits are 0.15-6.1ppb. This method has been applied to determination of trace metals of human hair.
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【References】
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【Co-references】
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