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《Journal of Analytical Science》 2001-01
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Determination of Hydrogen Peroxide by Micelle Electrochemiluminescence with Flow Injection Analysis

ZHANG Guo fang, CHEN Hong yuan  (Department of Chemistry, Institute of Analytical Science, Nanjing University, Nanjing, 210093)  
A fast and simple electrochemiluminescence (ECL) method for flow injection analysis of hydrogen peroxide in the system of 0.80 mol/L KCl containing 2.0×10 -3 mol/L Na 2CO 3 NaHCO 3 (pH 9.5) is presented, which is based on the electrogenerated reagent in situ at Pt anodic electrode applied by 1.3 V (vs. AgCl/Ag). The luminescence is produced at once when H 2O 2 is injected into this system. The ECL can be enhanced by Triton X 100 without any additional blank signal. And the response of ECL on concentration of H 2O 2 is linear in the range of 1.0×10 -7 ~1.0×10 -5 mol/L. The relative standard deviation of this method is 2.6% by 4.0×10 -7 mol/L H 2O 2 for 11 determinations, and the detection limit is 3.6×10 -8 mol/L. The proposed method for the determination of H 2O 2 is simple and practical, it has been successfully used for the determination of trace of H 2O 2 in rain water.
【Fund】: 国家自然科学基金 !( No. 2 97750 10 )
【CateGory Index】: O657.1;O611.62 ;
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