Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Analytical Science》 2012-01
Add to Favorite Get Latest Update

Determination of Sulfite in Dehydrated Vegetable by High Performance Liquid Chromatography with Post-Column Derivatization

PENG Xiao-jun,DENG Ai-hua,PANG Jin-shan(Xinhui Entry-Exit Inspection and Quarantine Bureau,Jiangmen 529100)  
A method was established for determinaton of sulfite in dehydrated vegetable by HPLC after reversed-phase silica gel column clean-up and post-column derivatization.The dehydrated vegetable sample was extracted with formaldehyde and was purfied by LC-C18 solid-phase extraction column.The separation was performed on a Discover ODS-C18 column with a mixture of tetrabutylammonium acid-acetonitrile as the mobile phase and 5,5′-dithiobis(2-nitrobenzoic acid) as the derivatization reagent.The detection wavelength was 445 nm.The linear range was 0.050~50.00 mg/L and the correlation coefficient was 0.9987.The limits of detection(S/N=3) and quantitation(S/N=10) of sulfite were 1 mg/kg and 2 mg/kg,respectively.The recoveries ranged from 62%~88% with the relative standard deviations less than 7.8% at spiked levels of 2~900 mg/kg.The method prevented the possibility of the false positive,and could meet the need of the practical measurement.
【CateGory Index】: O657.72;TS255.7
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【References】
Chinese Journal Full-text Database 8 Hits
1 Hao Yucui;Dept.of Environmental and Chemical Engineering,Key Laboratory of Micro-nano-material Preparation and Application of Tangshan City,Tangshan College;;Electrochemical behavior and determination of sulfite on Pt-Au nanoparticles/MWCNTs modified electrodes[J];化工新型材料;2016-03
2 LI Xiao-nan;ZHOU Yong-liang;CHEN Hong;SUN Yue;College of Traditional Chinese Medicine,Guangdong Pharmaceutical University;College of Chemistry and Chemical Engineering,Xiamen University;Pen-Tung Sah Institute of Micro-Nano Science and Technology,Xiamen University;;Rapidly detection of sulfur fumigated traditional Chinese medicine decoction pieces using surface-enhanced raman scattering spectroscopy[J];分析试验室;2016-01
3 YU Feng-jiao;ZHANG Xue-mei;LIU Si-ning;Donggang Entry-exit Inspection and Quarantine Bureau;National Key Laboratory of Pesticide and Veterinary Drug Residue and Marine Biotoxin Detection;;Determination of Sulphite Residue in Seafood by Ion Chromatography[J];辽东学院学报(自然科学版);2015-03
4 JI Lin;LI Dongxiang;PENG Ying;TONG Ling;School of Pharmacy,Shenyang Pharmaceutical University;Tasly Pharmaceutical Analysis Institute,Tianjin Tasly Group Co. ,Ltd.;;Advances in Study of Sulfur Dioxide Residue in Traditional Chinese Medicine and its Prepared Slices[J];中国现代中药;2015-02
5 Li Xuelian;Yang Li;Chen Hongping;Li Min;Liu Youping;State Key Laboratory Breeding Base of Systematic Research,Development and Utilization of Chinese Medicine Resources,Pharmacy college,Chengdu University of Traditional Chinese Medicine;;Progress in the Research of Sulfites in the Food[J];亚太传统医药;2015-03
6 LIU Jing;WANG Meiyan;FAN Shihua;Research Center for Analytical Science,Northeastern University;;Determination of Sulfur Dioxide in Wine by Gas Diffusion Separation-Sequential Injection Spectrophotometry[J];中国无机分析化学;2014-04
7 Hao Yucui;Dept.of Environmental and Chemical Engineering,Tangshan College;College of Environmental and Energy Engineering,Beijing University of Technology;;Voltammetric Determination of Sulfite Using Platinum Particle Modified Electrodes[J];广东化工;2014-13
8 YANG Juan;ZHANG Li;ZHU Wan-yan;DONG Li-jun;Linyi Entry-Exit Inspection and Quarantine Bureau;;Analysis of Determination Methods of Sulfite in Food[J];食品与药品;2014-02
【Citations】
Chinese Journal Full-text Database 4 Hits
1 HUANG Kai1,GAO Jun-yong2,MO Hai-tao3,LU Jia-jiong2,3,,FENG Bin-chao2,WU Jin-liang2(1.Guangxi Vocational & Industry Technical Institute,Nanning 530001,Guangxi,China;2.College of Light Industry and Food Engineering,Guangxi University,Nanning 530004,Guangxi,China;3.Research Center of Sugar Engineering,Guangxi University,Nanning 530004,Guangxi,China);DETERMINATION OF SULFITE IN PRESERVED BY ION CHROMATOGRAPHY[J];食品研究与开发;2009-09
2 HUANG Hui-ling,WANG Yu-jian,ZHUO Hai-hua,LIU Hong-zhuan,XU Li,JI Shao-fan,ZENG Min and LIN Zheng-feng(Technological Center,Hainan Entry-Exit Inspection and Quarantine Bureau,Haikou 570105);Determination of sulfite in food by ion chromatography[J];分析试验室;2009-08
3 ZHANG Shuang-ling1,ZHAO Kui-hao1,ZHOU De-qing2,LI Ying1(1.College of Food Science & Engineering,Laiyang Agricultural College,Qingdao 266109;2.National Center for Quality Supervision & Test of Aquatic Products,Qingdao 266071);Research of sulphites in aquatic products and residue determine[J];食品科技;2007-05
4 WU Fengwu, HE Zhike, LUO Qingyao, ZENG Yune (Department of Chemistry, Wuhan University, Wuhan, 430072);The Progress of Sulfur Dioxide Analysis[J];分析科学学报;2000-03
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 SHI Wenzhuang;HU Jing;LI Feng;Technology Center, China Tobacco Guangdong Industrial Co., Ltd.;;Simultaneous determination of anions of four acids in reconstituted tobacco[J];烟草科技;2016-06
2 Wang Zhihong;Su Yuanke;Li Chungang;Luo Xiao;Longkou Entry-Exit Inspection and Quarantine Bureau;;Preparation and Application of Proficiency Testing Matrix for Sulfites in Preserved Fruit[J];检验检疫学刊;2015-06
3 YU Feng-jiao;ZHANG Xue-mei;LIU Si-ning;Donggang Entry-exit Inspection and Quarantine Bureau;National Key Laboratory of Pesticide and Veterinary Drug Residue and Marine Biotoxin Detection;;Determination of Sulphite Residue in Seafood by Ion Chromatography[J];辽东学院学报(自然科学版);2015-03
4 WANG Jinxia;LIN Jiangli;LU Yi;WANG Jide;Key Laboratory of Oil and Gas Fine Chemicals Ministry of Education and Xinjiang Uyghur Autonomous Region,College of Chemistry and Chemical Engineering,Xinjiang University;Xinjiang Supervision and Inspection Institute for Product Quality;;Determination of Total Sulfite in Xinjiang Specialty Raisin by Fluorescence Derivatization[J];食品科学;2016-04
5 Jianyang ZHANG;Guoqing WANG;Shouzhen JIN;Guicen MA;Liyan CHEN;Xin LIU;Chengyin LU;The Laboratory for Tea Safety Risk Assesment of Ministry of Agriculture,Tea Research Institute,Chinese Academy of Agricultural Sciences;;Detection of SO_2 Residual in FLOS CHRYSANTHEMI by Accelerated Solvent Extraction/Ion Chromatography[J];Medicinal Plant;2015-Z2
6 Li Xuelian;Yang Li;Chen Hongping;Li Min;Liu Youping;State Key Laboratory Breeding Base of Systematic Research,Development and Utilization of Chinese Medicine Resources,Pharmacy college,Chengdu University of Traditional Chinese Medicine;;Progress in the Research of Sulfites in the Food[J];亚太传统医药;2015-03
7 GUO Chang-hong;XIA Ze-min;TAN Jian-hua;LI Hui-yong;XI Shao-feng;WANG Ji-cai;XIONG Xiao-ting;ZHAO Tian-tian;Guangzhou Quality Supervision and Testing Institute;;Determination of sulfite content in toothpaste by ion chromatography[J];日用化学工业;2014-07
8 SHAO Hong-hong;ZHOU Xiu-jin;ZHOU Xiang-yang;WAN Jing;FU Mi ni;Zhoushan Entry Exit Inspection and Quarantine Bureau;;Analysis of determination methods and results of sulfite in aquatic products[J];中国卫生检验杂志;2014-12
9 ZHANG Jian-yang;CHEN Li-yan;MA Gui-cen;LIU Xin;Tea Quality and Supervision Testing Center,Ministry of Agriculture,Tea Research Institute,Chinese Academy of Agricultural Sciences;;Determination of Sulfur Dioxide Residue in Chrysanthemum by Ion Chromatography after Accelerated Solvent Extraction[J];分析测试学报;2014-05
10 CHEN Guo-rong;Xinhui District Center for Disease Prevention and Control;;Determination of sulfite content in food by steam distillation-ion chromatography[J];中国卫生检验杂志;2014-04
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 LIU Peipei;HAN Xiaoxia;ZHAO Bing;XU Weiqing;WANG Xu;State Key Laboratory of Supramolecular Structure and Materials,Jilin University;;Surface-enhanced Raman Scattering-based Diquat Detection[J];高等学校化学学报;2015-08
2 WANG Yong-qing;LI Duo;WANG Shuo-nan;LIU Xin-xin;LIU Yu-fei;Electronic Information Engineering College of Hebei University,Key Laboratory of Digital Medical Engineering of Hebei Province;First Central Hospital in Baoding,Dispensary for Western Medicine;;Research on portable device for rapid detection of sulfur residue in honeysuckle[J];分析试验室;2015-07
3 SUN Xu-dong;DONG Xiao-ling;School of Mechatronics Engineering,East China Jiaotong University;School of Foreign Language,East China Jiaotong University;;Quantitative Analysis of Dimethoate Pesticide Residues in Honey by Surface-Enhanced Raman Spectroscopy[J];光谱学与光谱分析;2015-06
4 Wan Lingyan;Li Fuxian;Luo Yan;;The Effect of Sulphite in Foods and the Factors Affecting Detection of Pararosaniline Hydrochloride Method[J];计量与测试技术;2015-03
5 Wu Erka;Bo Zheng;Hu Dan;Ma Wei;Wang Zhihua;Zhu Weiguang;Yan Jianhua;Cen Kefa;State Key Laboratory of Clean Energy Utilization,Institute for Thermal Power Engineering,Zhejiang University;;Pulse electrodeposition of Pt on vertical oriented graphene as catalysts for DMFCs[J];化工新型材料;2015-02
6 GUO Kun;CHEN Xin;YE Lin;CHEN Su-hong;Department of Occupational and Environmental Health,School of Public Health,Jilin University;Beijing Key Laboratory of New Molecular Diagnosis Technologies for Infectious Diseases,Beijing Institute of Radiation Medicine;;Sensitive surface-enhanced Raman spectroscopy detection of thiram based on hybrid substrate[J];军事医学;2015-01
7 Huang Shanshan;Li Zhonghai;Li Jilie;Guo Xiaobing;Geng Mei;Central South University of Forestry and Technology,National Engineering Laboratory of Food Deep Processing;;Research progress of gold nanoparticles applied in electrochemical biosensors[J];化工新型材料;2014-06
8 ZHANG Jian-yang;CHEN Li-yan;MA Gui-cen;LIU Xin;Tea Quality and Supervision Testing Center,Ministry of Agriculture,Tea Research Institute,Chinese Academy of Agricultural Sciences;;Determination of Sulfur Dioxide Residue in Chrysanthemum by Ion Chromatography after Accelerated Solvent Extraction[J];分析测试学报;2014-05
9 LUO Jian-min;WANG Ai-xia;CHEN Jun-yu;Xinjiang Uygur Autonomous Region Academy of Instrument Analysis;;Determination of Sulfur Dioxide in Raisins by Ion Chromatography[J];食品研究与开发;2014-04
10 JIA Zheng-wei;MAO Bei-ping;MIAO Shui;MAO Xiu-hong;JI Shen;Shanghai Institute for Food and Drug Control;;Determination of sulfur dioxide residues in sulfur fumigated Chinese herbs with headspace gas chromatography[J];药学学报;2014-02
【Secondary References】
Chinese Journal Full-text Database 7 Hits
1 LI Xue-mei;CHEN Ying;ZHANG Xue-mei;YU Feng-jiao;National Key Laboratory of Pesticide and Veterinary Drug Residue and Marine Biotoxin Detection;Donggang Entry -exit Inspection and Quarantine Bureau;;Detection of Polyphosphates in Aquatic Products by Ion Chromatography[J];辽东学院学报(自然科学版);2016-03
2 HU Mi;SU Xiaochun;HE Bing;CHENG Yan;SHI Chaoou;College of Chemistry and Molecular Engineering, East China University of Science and Technology;Changzhou Fangyuan Pharmaceutical Co., Ltd.;;Determination of Sodium Sulfite in Etimicin Sulfate Injection by Ion Chromatography[J];中国医药工业杂志;2016-05
3 WANG Na-Ni;FEI Ying;WANG Xu-Ping;SHOU Dan;ZHU Yan;Department of medicine,Zhejiang Academy of Traditional Chinese Medicine;Department of Chemistry,Zhejiang University;;Application studies of the analysis of traditional Chinese medicine by ion chromatography[J];食品安全质量检测学报;2015-12
4 ZHAO Miao-miao;LI Ru;LI Han-lin;LI Fei-yang;School of Environmental and Chemical Engineering,Xi'an Polytechnic University;;Study on breeding of efficient desulfurization bacteria muted by low temperature plasma[J];应用化工;2016-02
5 YANG Shu-yun;BAI Jian-ying;ZHANG Yan;WANG Pan;LIU Yan-fei;Department of Environmental Health,School of Public Health,Shanxi Medical University;;Effects of sodium sulfite on damage and expression of necroptosis- associated protein-receptor interacting protein 1(RIP1) in HL-7702 cells[J];环境与健康杂志;2015-12
6 TAN Ting-ting;WANG Ying;OU Shi-yi;TENG Jiu-wei;Department of Food Science and Engineering,Jinan University;;Oxidation of As(Ⅲ) and its kinetic analysis in high pressure cooking model[J];食品与发酵工业;2015-12
7 HAO Yucui;LI Ai;Department of Environmental and Chemical Engineering,Tangshan College;;Determination of sulfite using Pt-Fe(Ⅲ) and multi-walled carbon nanotubes modified electrodes[J];中国测试;2015-07
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 ZHANG Shuang-ling1,ZHAO Kui-hao1,ZHOU De-qing2,LI Ying1(1.College of Food Science & Engineering,Laiyang Agricultural College,Qingdao 266109;2.National Center for Quality Supervision & Test of Aquatic Products,Qingdao 266071);Research of sulphites in aquatic products and residue determine[J];食品科技;2007-05
2 WU Wei-ping~1,ZHANG Lei~1,LI Jie~1,PENG Shao-jie~1,ZHAO Yu-xiang~1,WANG Hua~2(1.Shanghai Institute of Food and Drug Supervision,Shanghai 200021,China;2.Shanghai Nutritions Food Quality Surveillance and Inspection Center,Shanghai 200082,China);Study on method for rapid detection of residual sulfur dioxide in food[J];上海预防医学杂志;2006-09
3 Zou Yueli;Measurement of sulfite in garlic by ion exchange chomatography[J];食品工业科技;2006-08
4 CHEN Fei-dong, DAI Zhi-yuan (The College of Food Science,Biotechnology&Environmental Engineering, Zhejiang Gongshang University, Hangzhou 310035, Zhejiang, China);THE PROGRESS OF SULFITE ANALYSIS IN FOOD PRODUCTS[J];食品研究与开发;2006-08
5 GUO Li-ping1,MO Hai-tao2,LU Jia-jiong1,2,WU Jin-liang1(1.Light Industry and Food Engineering Institute,Guangxi Univerisity,Nanning 530004;2.Research Center of Sugar Engineering,Guangxi University,Nanning 530004);Measurement of sulfite in hemerocallis citrina baroni by ion chromatography[J];食品科技;2006-05
6 Mo Haitao~1 Guo Liping~2 Li Yongku~1 1(Engineering Center for Sugar Cane and Cane Sugar,Guangxi University,Nanning 530004,China) 2(Light Industry and Food Engineering Institute,Guangxi University,Nanning 530004,China);Determination of Sulfur Dioxide in Sugar by Ion Chromatography[J];食品与发酵工业;2006-02
7 ZHOU De-qing1,ZHANG Shuang-ling1,2,XIN Sheng-chang1(1.Yellow Sea Fisheries Research Institute,China Fisheries Science Academy,Qingdao 266071,China;2.Northwest Sci-Tech University of Agriculture and Forestry,Yangling 712100,China);Review on the Function and Application of Sulphite in Food Processing[J];食品科学;2004-12
8 MENG Zi-qiang, RAI Wei. Institute of Environmental Medicine and Toxicology, Shanxi University, Taiyuan, Shanxi 030006, China;Oxidation Damage of Sulfur Dioxide Inhalation on Testicles of Male Mice[J];环境与健康杂志;2003-02
9 LI Ying,WANG Cheng-yun (Shenzhen Entry-Exit Inspection and Quarantine Bureau, Shenzhen 518045, China);Determination of sulfites in foods[J];湘潭师范学院学报(自然科学版);2001-01
10 Liu Zhe Liu Kena Song Qiang Mou Shifen(Research Center for Eec-Environmental Sciences, Chinese Academy of Sciences,Beijing, 100085 );Determination of Sulfite in Food by Exclusion Ion Chromatography with Pulsed Amperometric Detection[J];食品与发酵工业;1997-04
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved