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《Journal of Analytical Science》 2012-01
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A HPLC-CL Method for the Determination of Residual Sudan Ⅰ in Food

YUAN Yi-qin,ZHU Zhi-jia,REN Yi-zhen,ZHANG Wei(College of Chemistry,Chemical Engineering and Biotechnology, Donghua University,Shanghai 201620)  
A new analytical method of high performance liquid chromatography chemiluminescence(HPLC-CL) for Sudan Ⅰ is established based on the sensitizing effect of Sudan Ⅰ on luminol-KIO4 system under alkaline condition.A Phenomenex C18 column(250×4.6 mm,5 μm) as separation column and acetonitrile-methanol-water(5∶4∶1 V/V/V) as mobile phase was used throughout the experiment.The results show that a good linear relationship exists between the CL intensity and the concentration of Sudan Ⅰ in the range of 0.001~0.50 μg·mL-1(R=0.9996).The detection limit is 5 ng·kg-1 and the relative standard deviation is 1.45%(c=0.01 μg·mL-1,n=6).The recovery is in the range of 95.0%~104.0%.This method has been proved to be simple,sensitive and accurate,and it has been applied to determine Sudan Ⅰ with satisfactory results.
【CateGory Index】: O657.72;TS207.5
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【Citations】
Chinese Journal Full-text Database 3 Hits
1 WU Yin-Liang1,3,LI Cun2,LIU Yong-Jun3,JIANG Yan-Bin3,LIU Xing-Guo3,SHEN Jian-Zhong1 1(College of Veterinary Medicine,China Agricultural University,Beijing 100094)2(College of Agriculture,Hebei University of Engineering,Handan 056038)3(China Animal Disease Control Center,Beijing 100026);Fast Determination of Sudan Dyes in Duck Meat and Egg by High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2008-06
2 WANG Peng1,2, GUO Shaofei3, JING Tao1, HU Xiaozhong2, LIN Yanfei2, LUO Jing2, SONG Qi2, ZHOU Yikai1, MEI Surong1 (1.Institute of Environmental Medicine, School of Public Health, Tongji Medical College, Huazhong University of Science and Technology, Key Laboratory of Environment & Health of Ministry of Education, Wuhan 430030, China; 2.Hubei Entry-Exit Inspection and Quarantine Bureau, Wuhan 430022, China; 3.Pharmacy College, Tongji Medical College, Huazhong University, Wuhan 430030, China);Determination of Sudan Red dyes in eggs using liquid chromatography-tandem mass spectrometry and matrix solid-phase dispersion technique[J];Chinese Journal of Chromatography;2008-03
3 YAO Jin-wen,FENG Xin-chang(Gansu Center for Disease Control and Prevention,Lanzhou 730000);HPLC analysis of Sudan dyes in chili spices[J];Chinese Journal of Health Laboratory Technology;2010-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 CHAI Yi-feng*,ZHU Zhen-yu and CHEN Xiao-fei(Department of Pharmaceutical Analysis,School of Pharmacy,Second Military Medical University,Shanghai 200433),Fenxi Shiyanshi,2010,29(9):78~122;Pharmaceutical analysis(I)[J];Chinese Journal of Analysis Laboratory;2010-09
2 Zhou Fangmei1,Cai Jizhi2,Ma Fengli2,Cai Shuanfu1(1.Guangdong Food Quality Supervision and Inspection Station,Guangzhou 510308;2.Guangdong Food Industry Institution,Guangdong Provincial Public Laboratory of Food Industry,Guangzhou 510308,China);Determination of Sudan Deys in Lipstick[J];Guangdong Chemical Industry;2009-04
3 ZHOU Jian-ke,LIU Rui-ying,LI Xiao-yang(Research Center of Physics and Chemistry Analysis,Hebei University; Hebei Province Key Laboratory of Analytical Science and Technology,Baoding 071002,China);Determination of SudanⅠand Ⅲ in Hawthorn Maltose by High Performance Liquid Chromatography[J];Modern Food Science and Technology;2009-02
4 FAN Xiao-li1,2,DONG Ying1,ZOU Ming-qiang2,QI Xiao-hua2,ZHANG Xiao-fang2,CHEN Yan2(1.Jiangsu University,Zhenjiang 212013,China;2.Chinese Academy of Inspection and Quarantine,Beijing 100123,China);Study on Significantly Differences of Endogenous Metabolites in Eggs which Obtained from Layers Fed with Sudan Ⅳ[J];China Animal Husbandry & Veterinary Medicine;2011-12
5 FAN Wen-Rui,WU Qing,LAO Yang,LU Yu-Shan(College of Food Science,South China Agricultural University, Food Quality and Safety Key Laboratory of Guangdong Province,Guangzhou 510642);Determination of Seven Inedible Pigments in Food Using High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2012-02
6 Wei Nannan,Mao Hui,Wu Li,Lu Tianhong,Zhao Bo,Du Jiangyan(Jiangsu Key Laboratory of Biofunctional Materials,School of Chemistry and Environmental Science,Nanjing Normal University,Nanjing 210046,China);Electrochemical Study on Interaction of SudanⅡ and Hemoglobin[J];Journal of Nanjing Normal University(Natural Science Edition);2010-01
7 DAI Qing,WANG Yan,BAO Xuewei,JING Tao,HAO Qiaoling,ZHOU Yikai,MEI Surong(Key Laboratory of Environment & Health of Ministry of Education,Institute of Environmental Medicine,School of Public Health,Tongji Medical College,Huazhong University of Science and Technology,Wuhan 430030,China);Preparation and evaluation of Sudan Red Ⅰ molecularly imprinted polymer[J];Chinese Journal of Chromatography;2009-06
8 SONG Yong-qing,LI Ying-ying,ZHAO Rong (China Meat Food Research Center,Beijing 100068);Determination of Sudan Red in eggs by UPLC-MS/MS[J];Science and Technology of Cereals,Oils and Foods;2009-06
9 Yang Minli,Gu Wancheng,Chu Xiaogang,Wang Daning (Institute of Food Safety,Chinese Academy of Inspection and Quarantine,Beijing 100123);Characterization and Rebinding Property of Molecularly Imprinted Polymers with Salbutamol as Template[J];Modern Scientific Instruments;2011-01
10 DENG Guang-hui,CHEN Sheng-yu,ZHANG Gui-hua (Ecological Project Institute,Guangxi University for Nationalities,Nanning 530006,China);Determinnation of Sudan I by capillary electrophoresis with amperometric detection[J];China Condiment;2011-04
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 XIA Hong-yu~1,DAI Zheng-mang~2(School of Chemistry and Environmental Science,Anqing Teachers College,Anqing 246011,China);The Poison Mechanism and Calibaration Method of Sudan[J];Journal of Anqing Teachers College(Natural Science Edition);2005-04
2 Li Yueqi, Yao Jianguo, Hashi Yuki. Beijing Analysis Center, Shimadzu International Trade, shanghai co., Beijing 100020, China;Detection of Magdala in Food Through High Performance Liquid Chromatography[J];Chinese Journal of Frontier Health and Quarantine;2006-02
3 Liang Jingbo(Environmental Monitoring Station of Zibo,Zibo 255040,China)Huang Jinyan(Food Security Monitoring Center of Zibo,Zibo 255040,China);DETERMINATION OF RED DYESTUFFS OF SUDAN IN THE CHILLI SAUCE BY INVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY[J];Chemical Analysis and Meterage;2005-05
4 HUANG Hong-Nan, HUA Yong-You, LIN Hong-Lin, et al(Fujian Center for Disease Control and Prevention, Fuzhou 350001, China);Research on the Rapid Determination of the Sudan in the Polluted Food by HPLC-PDA-MS[J];Strait Journal of Preventive Medicine;2005-04
5 Wang Na,Cui Jiantao,Pan Zhili,Wang Yanmin,Ai Zhilu (Food Science and Technology College,He'nan Agricultural University,Zhengzhou 450002,China);Comparison of European Union Law and GB Code Law about Determining Sudan in Food[J];Academic Periodical of Farm Products Processing;2006-12
6 HAN Jin-song,XU Ming-xia,CHEN Zhan.(Foshan Municipal Center for Disease Control and Prevention,Foshan 528000,Guangdong,P.R.China);Study on the detection of Sudanhong from foods by using high performance liquid phase chromatography[J];China Tropical Medicine;2006-07
7 ZHENG Mingming,WU Jianhong,LUO Dan,YU Qiongwei,FENG Yuqi(College of Chemistry and Molecular Sciences,Wuhan University,Wuhan 430072,China);Determination of Sudan Red Dyes in Hot Chili Products by Humic Acid-Bonded Silica Solid-Phase Extraction Coupled with High Performance Liquid Chromatography[J];Chinese Journal of Chromatography;2007-05
8 DU Zhenxia,SUN Shuqi(Beijing University of Chemical Technology,Beijing 100029,China);Determination of Sudan Red Ⅰ-Ⅳ in Duck Egg Yolk Using Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry[J];Chinese Journal of Chromatography;2007-05
9 WANG Quanlin,SHI Pingping,ZHANG Shufen,SHEN Jian,FU Xiao(Supervision and Inspection Institute of Product Quality,Ningbo 315041,China);Simultaneous Determination of Canthaxanthin and Sudan Red in Salted Duck Egg Yolk by Reversed-Phase High Performance Liquid Chromatography[J];Chinese Journal of Chromatography;2007-06
10 WANG Jun(Shandong Institute of Product Quality supervision and Inspection,Jinan 250100,China);The determination of sudan dyes in foods by HPLC-Mass[J];JOURNAL OF SHANDONG INSTITUTE OF LIGHT INDUSTRY(NATURAL SCIENCE EDITION);2005-04
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