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《Chinese Journal of Analysis Laboratory》 2011-03
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Molecularly imprinted on-line solid-phase extraction combined with chemiluminescence for the determination of resveratrol

SHI Zuo-long1,ZHANG Zhu-jun2,TANG Hong1,ZHAO Qiong1,YANG Xi1 and CHEN Yu1(1.Institute of Industrial Hygiene of Ordnance Industry,Xi'an 710065;2.School of Chemistry and Materials Science;Shaanxi Normal University,Xi'an 710062)  
The molecularly imprinted particles were synthesized using resveratrol as the template.As a solid-phase extraction micro-column,a polytetrafluoroe-thylene tube was connected to the sampling loop of the eight-way injection valve for the preconcentration and extraction of resveratrol.The eluent was used as the carrier to extract the adsorbed resveratrol and then reacted with potassium permanganate in the flow cell to produce CL.The chemiluminescence intensity is correlated linearly with resveratrol concentration in the range of 2.5×10-7～6.1×10-5 g/mL with a detection limit of(3σ) 8×10-6 g/mL.The relative standard deviation is 2.0% for 1.5×10-6 g/mL of resveratrol(n=11).
【Key Words】： Molecularly imprinted polymer Chemiluminescence Resveratrol
【Fund】： 国家自然科学基金项目(30470886)资助
【CateGory Index】： O657.3;TS262.6
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