Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chinese Journal of Analysis Laboratory》 2011-08
Add to Favorite Get Latest Update

Molecularly imprinted solid phase extraction coupled with high performance liquid chromatography for the simultaneous determination of cyromazine and melamine residues in chicken plasma

WEI Yan-ling,ZHANG Jia-hui,HE Qian-qian,ZHANG Gao-kui,WANG Xu-feng and HE Li-min(Department of Pharmacology and Toxicology,College of Veterinary Medicine,South China Agricultural University,Guangzhou 510642)  
A high performance liquid chromatographic method based on molecularly imprinted solid-phase extraction for the simultaneous determination of cyromazine(CYR) and melamine(MEL) residues in chicken plasma was developed.Molecularly imprinted polymers with high selectivity to CYR and MEL were prepared using CYR as a template,methacrylic acid as monomer,ethylene glycol dimethacrylate as cross-linker.The characteristics and solid phase extraction conditions of the molecularly imprinted polymers as adsorptive material for the selective extraction and enrichment of CYR and MEL were evaluated.The plasma sample was precipitated by 1% trichloroacetic acid solution,further cleaned up using the molecularly imprinted solid-phase extraction cartridge.An obvious ultraviolet absorbance at wavelength of 240 nm was observed when CYR and MEL were in the system of sodium octanesulfonate(pH 3.0) buffer-acetonitrile(82:18,V/V).Therefore,the two analytes were determined by ion-pair reversed phase HPLC.The method had good linearity in the range of 0.10-10.0 μg/mL for two anayltes.The obtained recoveries were above 70% with the relative standard deviations of less than 10% for both CYR and MEL.The limits of detection of CYR and MEL in chicken plasma were ca.0.05 μg/mL.
【Fund】: 农业行业标准制定专项(070106-69)资助
【CateGory Index】: R155.5
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 4 Hits
1 Wang Hui1,2,3,Dong Yuanhua1,2,3,An Qiong1,2(1.State Key Laboratory of Soil and Sustainable AgricultureI,nstitute of Soil Science,Chinese Academy of Sciences,Nanjing,210008,China;2.Institute of Soil Science,Chinese Academy of Sciences – Hong Kong Baptist University(ISSAS-HKBU) Joint Laboratory on Soil and Environment,Nanjing,210008,China;3.Graduate School,Chinese Academy of Sciences,Beijing 100039,China);Research advance in biotoxicology and environmental behavior of cyromazine[J];Transactions of the Chinese Society of Agricultural Engineering;2008-01
2 ZHOU Wen-hui1,2,LIN Li-ming3,GUO Xiu-chun1,2,YANG Huang-hao2,WANG Xiao-ru1,2(1.College of Chemistry and Chemical Engineering,Ocean University of China,Qingdao 266100,China;2.The First Institute of Oceanography,State Oceanic Administration,Qingdao 266061,China;3.Shandong Entry-Exit Inspection & Quarantine Bureau,Qingdao 266001,China);Synthesis of Melamine Molecularly Imprinted Polymer and Separation of Melamine in Milk Products[J];Journal of Instrumental Analysis;2009-06
3 TANG Ling-li 1,2,3, WANG Hui 2,3, DONG Yuan-hua 2,3, LIU De-hui 1, ZHAO Ling 2,3, ZHANG Jing-qiang 2,3, LIU Xing-cheng 2,3, AN Qiong 2,3 (1 Nanjing Agricultural University, Nanjing 210095, China; 2 State Key Laboratory of Soil and Sustainable Agriculture(Institute of Soil Science, Chinese Academy of Sciences), Nanjing 210008, China; 3 Institute of Soil Science, Chinese Academy of Sciences – Hongkong Baptist University (ISSAS-HKBU) Joint Laboratory on Soil and Environment, Nanjing 210008, China);Determination of Cyromazine and Melamine in Soils by High-performance Liquid Chromatographic Method[J];Soils;2009-05
4 HE Li-min1,LIU Kai-yong2,WU Li1,ZHENG Ya-qiu1,GUO Hong-bin1,ZHANG Qing-jie1,ZENG Zhen-ling1(1.College of Veterinary Medicine,South China Agricultural University,Guangzhou 510642;2.College of Food and Bioengineering,Henan University of Science and Technology,Luoyang,Henan 471003;China);Molecularly Imprinted Polymer Solid Phase Extraction Coupled with Gas Chromatography-Mass Spectrometry for the Determination of Melamine in Eggs[J];Chinese Journal of Veterinary Drug;2011-01
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 ZHAO Shuo,CUI Li-feng,SHEN Qing(College of Chemical and Environmental Engineering,Beijing Technology and Business University,Beijing 100048,China);DETERMINATION OF MELAMINE IN LIQUID MILK BASED ON MOLECULARLY IMPRINTED ELECTROCHEMICAL SENSORS[J];Journal of Beijing Technology and Business University(Natural Science Edition);2010-06
2 HU Yu-li1,HE Yi-gang1,MI Zi-you1,LIU Han-ru2,SU Liang1(1.Chongqing Institute of Veterinary Drugs and Feed,Chongqing,401120,China;2.College of Pharmacy,Southwest University,Chongqing,400715,China);Application of Molecular Imprinting Technique in Veterinary Drug Residue Analysis[J];Progress in Veterinary Medicine;2011-01
3 YANG Weihai,YAN Shoulei,WEI Chen,WANG Qingzhang(Huazhong Agricultural University,College of Food Science and Technology,Wuhan 430070);PREPARATION OF MELAMINE MOLECULARLY IMPRINTED POLYMER MICROSPHERES BY PRECIPITATION POLYMERIZATION[J];Acta Polymerica Sinica;2010-10
4 Chi Damin Su Liqiang Deng xishan Wang Lili(College of Chemistry and Chemical Engineering,Qiqihar Uiniversity,Helongjiang Qiqihar 161006);Development in the Research of the Selection Methods of Functional Monomer in Molecular Imprinting[J];Chemical Industry Times;2009-12
5 WANG Shuo,LIU Xiao-jun,LIANG Zhen-cai,WANG Peng(Technical Center of Heilongjiang Entry-Exit Inspection and Quarantine Bureau,Harbin 150000,China);Tandem Mass Spectrometry of High-fat Cooked Food of Air Craft by One High-Performance Liquid Chromatography[J];Journal of Heihe University;2010-03
6 TANG Ling-li~(1,2,3),WANG Hui~(1,2),DONG Yuan-hua~(1,2),LIU De-hui~3,ZHAO Ling~(1,2),ZHANG Jing-qiang~(1,2),(LIU Xing-cheng~(1,2),) AN Qiong~(1,2)(1.State Key Laboratory of Soil and Sustainable Agriculture,Institute of Soil Science,Chinese Academy of Sciences,Nanjing 210008,China;2.Joint Laboratory on Soil and Environment,Institute of Soil Science,Chinese Academy of Sciences-Hongkong Baptist University(ISSAS-HKBU),Nanjing 210008, China;3.College of Resources and Environmental Sciences,Nanjing Agricultural University,Nanjing 210095,China);Adsorption of Cyromazine on Five Typical Soils in China[J];Environmental Science;2009-10
7 HAN Dong-fang~1,2,WANG De-han~2,HUANG Pei-zhao~1,DUAN Ji-xian~1,GE Ren-shan~1,LIU Ming-jiang~1(1.Shenzhen Batian Ecotypic Engineering Co.Ltd.,Shenzhen 518105,China;2.College of Nature Resources and Environment,South China Agricultural University,Guangzhou 510642,China);Effect of the Melamine Residue in Soil on Growth of Chinese Cabbage[J];Environmental Science;2010-03
8 WANG Zhong-dong~1,BAI Wen~1,WANG Yan-hong~2,WANG Shi-cheng~2,LIN Gui-feng~2 (1.College of Light Industry and Economics&Management,Jilin University,Changchun 130062,China; 2.Institute of Applied Ecology,Chinese Academy of Sciences,Shenyang 110015,China);Application of Molecular Imprinting Technology in Food Safety Detection and Analysis[J];Journal of Inner Mongolia University for Nationalities(Natural Sciences);2011-02
9 Lv Ruihe1,Wan Zhengkai2,He Juan1 (1.School of Chemistry and Chemical Engineering,He nan University of Technology,Henan Zhengzhou 450001,China;2.College of Science,Henan Agricultural University,Henan Zhengzhou 450001,China);Application of Molecular Imprinting Solid Phase Extraction Technique in Food Safety Detection[J];Sichuan Chemical Industry;2010-01
10 ZHANG Xi,JIN Fen,QIAN Yong-zhong,WANG Jing(Institute of Quality Standards & Testing Technology for Agro-Products,Chinese Academy of Agricultural Sciences,Beijing 100081,China);Review on advance of melamine in foods and animal feeds[J];Science and Technology of Food Industry;2009-07
China Proceedings of conference Full-text Database 1 Hits
1 ;The effect of melamine on the function of male Beagles' kidney and testis[A];[C];2009
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Wang Zheng (Fujian Provincial Central Inspection Institute,Fuzhou 350002,China);Determination of Melamine and the Related Analogs in Animal Food by Gas Chromatography-Mass Spectrometry[J];Fujian Analysis & Testing;2008-02
2 Lai Jiaping, He Xiwen *, Guo Hongsheng (Department of Chemistry, Nankai University, Tianjin 300071) Liang Hong (Chemistry and Life College, Guangxi Normal University, Guilin 541004);A Review on Molecular Imprinting Technique[J];Chinese Journal of Analytieal Chemistry;2001-07
3 Wang Pei-Long, Fan Li, Song Rong, Gao Sheng, Su Xiao-Ou, Yang Shu-Ming(Institute of Quality Standards and Testing Technology for Agricultural Products,China Agricultural Academy of Science, Beijing 100081);Molecularly Imprinted Polymer Solid Phase Extraction Coupled with Gas Chromatography-Mass Spectrometry for the Determination of Trace Clenbuterol Hydrochloric in Animal Urine[J];Chinese Journal of Analytical Chemistry;2007-09
4 LI Yong-qing, WANG Jun (Shandong Lianmeng Chemicals Ltd.co.,Shouguang 262700,China);Application and Production of Cyanuramide[J];Chemial Technology Market;2004-05
5 GUO Yun MO Han hong AN Feng chun LI Jian zhong ZHENG Ming hui (Research Center for Eco Environmental Sciences,Chinese Academy of Sciences,Beijing,100085);RESIDUE ANALYTICAL METHOD OF CYROMAZINE IN CUCUMBER AND SOIL USING HPLC[J];Environmental Chemistry;2004-06
6 YANG-Fan~1,LIU Li~2,DAI Li-guang~1,LIU Chang-ying~1,WU Dong-mei~1,LIU Zhi-yong~1(1.Jiangxi Institute of Labour Hygiene and Occupational Medicine,Jiangxi Nanchang 330046 PRC;2.Jiangxi Institute of Parasitic Disease,Jiangxi Nanchang 330046 PRC);The Acute Toxicity and Dermal Sensitisation of 10% Cyromazine[J];Jiangxi Science;2006-06
7 PU Shi-jin, XU Xiao-yan (Vet Med Coll, Yangzhou Univ, Yangzhou, 225009, China);Determination of cyromazine residues in chicken tissues by high-performance liquid chromatography[J];Journal of Yandzhou University;2005-04
8 WU Mingli Ningxia DaRong chemical & metallurgy Co.LTD,Shizuishan,753001;Determination of melamine in cyanamide by high performance liquid phase chromatography (HPLC)[J];Mingxia Petroleum and Chemical Industry;2005-02
9 Wang Hui1,2,3,Dong Yuanhua1,2,3,An Qiong1,2(1.State Key Laboratory of Soil and Sustainable AgricultureI,nstitute of Soil Science,Chinese Academy of Sciences,Nanjing,210008,China;2.Institute of Soil Science,Chinese Academy of Sciences – Hong Kong Baptist University(ISSAS-HKBU) Joint Laboratory on Soil and Environment,Nanjing,210008,China;3.Graduate School,Chinese Academy of Sciences,Beijing 100039,China);Research advance in biotoxicology and environmental behavior of cyromazine[J];Transactions of the Chinese Society of Agricultural Engineering;2008-01
10 Wu Chunxian et al. (Department of Plant Protection Shandong Agricultural University,Tai′an 271018);Test on Control of Lirimyza sativae with 10% Cyromazine EC[J];Pesticides;2001-01
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved