Preparation and study of puerarin electrochemical sensor based on molecularly imprinted polymer--《Chinese Journal of Analysis Laboratory》2012年06期

《Chinese Journal of Analysis Laboratory》 2012-06

Preparation and study of puerarin electrochemical sensor based on molecularly imprinted polymer

WANG Lin1,TAN Xue-cai1,2,GONG Qi1,LIU Li2,ZHAO Dan-dan2,LEI Fu-hou2 and HUANG Zai-yin 2(1.School of Chemistry & Chemical Engineering,Guangxi University,Nanning 530004;2.School of Chemistry and Chemical Engineering,Guangxi University for Nationalities,Nanning 530008)

Using acrylamide as a functional monomer,puerarin as a template,maleic rosin acrylic acid glycol ester as the cross linking agent,molecularly imprinted polymer membrane is synthesized in solution by cyclic voltammetry.The sensor shows high selectivity and good sensitivity towards the target puerarin and it gives a linear correlation to puerarin concentration over a range from 6.0×10-8 to 1.6×10-3 mol/L with the detection limit of 2.0×10-8 mol/L.The sensor has been applied to the analysis of puerarin in puerarin injection and papaya﹠pueraria root tablet samples with recoveries ranging from 97.7% to 106.4%.

【Key Words】： Maleic rosin acrylic acid glycol ester Puerarin Molecularly imprinted polymer Electrochemical sensor
【Fund】：国家自然科学基金项目(21065001 30960306 21165003);; 广西自然科学基金项目(0991084 0991001Z);; 广西教育厅科研项目(200812MS074);; 广西林产化学品开发与应用重点实验室项目(GXFC08-06)资助
【CateGory Index】： TP212.2

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