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《Chinese Journal of Analysis Laboratory》 2012-09
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Preparation of parathion imprinted polymer and its application for the determination of parathion in water

LIU Jing,ZENG Xing-yu,LIU Xiao-qi,WANG Yi,ZHAO Xu-long,FENG Yan-hui and PAN Xian-hui(Institute of Seawater Desalination and Multipurpose Utilization,State Oceanic Administration,Tianjin 300192)  
In order to separate and concentrate the parathion in water efficiently,the molecularly imprinted polymer(MIP) was synthesized by photo-polymerization with parathion as the template molecule and TMPTA as a crosslinking agent.According to the UV and IR spectra,the interaction between parathion and functional monomers were studied and the MIP was evaluated.The above prepared MIP was used to extract parathion in water samples with SPE-GC,the detection limit(3S/N) was 0.48 μg/L.Recoveries were 86.2%～115.7 % and relative standard deviations(n=6) were 3.0%～6.6%.
【Key Words】： Molecularly imprinted polymer Photo-polymerization Parathion SPE-GC Water
【Fund】： 国家海洋局业务化项目(1511112000005);; 中央级公益性科研院所基本科研业务费专项资金项目(K-JBYWF-2010-G16)资助
【CateGory Index】： X832
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