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《Analytical Instrumentation》 2017-04
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Determination of 4-n-octyl phenol,4-n-nonyl phenol,nonyl phenol and bisphenol A in cosmetics by gas chromatography with mass spectrometry

Zhao Yanju;Li Qingqing;Hu Shoujiang;Shanghai Institute of Quality Inspection and Technical Research;  
The samples were extracted by methanol.Sample purification was performed on an UCT extraction column.The separation of four compounds was carried out on a DB-5ms column.The analytes were indentified with retention time and quantified by the external standard method.The calibration curves for the four compounds were linear in the range of 0-1000μg/L with the correlation coefficients more than0.99.The quantification limits of 4-n-octyl phenol and 4-n-nonyl phenol were 10μg/kg,nonylphenol was50μg/kg,and bisphenol A was 6.8μg/kg.The recoveries in emulsion and gel samples were in the range of 89.1%-102.7%.The method is accurate,fast and suitable for quantitative inspection of 4-n-octyl phenol,4-n-nonyl phenol,nonyl phenol and bisphenol A in emulsion and gel cosmetics.
【Key Words】: cosmetics GC-MS 4-n-octyl phenol 4-n-nonyl phenol nonyl phenol bisphenol A
【CateGory Index】: O657.63;TQ658
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