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《Journal of Functional Polymers》 2008-04
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Reactive Extrusion of 1,3,5-Trimethyl-1,3,5-Tris(3′,3′,3′-Trifluoropropyl) Cyclotrisiloxane Simulated in Haake Rheometer

JIANG Wei,GAO Ya-juan,ZHENG An-na,ZHOU Ying-jian,XU Xiang,HU Fu-zeng(School of Materials Science and Engineering,East China University of Science and Technology,Shanghai 200237,China)  
The anionic ring-opening polymerization of 1,3,5-trimethyl-1,3,5-tris-(3′,3′,3′-trifluoropro-pyl) cyclotrisiloxane was conducted in a Haake Rheometer.The fluorosilicone rubber obtained were characterized with GPC and FT-IR,1H-NMR.The study shows that polymer of M_n=2.45×105 can be obtained at 120 ℃ for 4 min in the presence of ethyl acetate.The effects of relevant process parameters such as temperature and reaction time on the anionic ring-opening polymerization of D_3F were studied as well.
【CateGory Index】: TQ316.3
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