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《Chinese Journal of Spectroscopy Laboratory》 2010-02
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Spectroscopy Study on Molecular Recognition of 1-Naphthalenamine Molecularly Imprinted Polymer

TANG Wen-Wen YANG Jun XU Ying-Boa WANG Cheng-Huia CAI Ji-Bao SU Qing-De(Research Center of Tobacco and Health,University of Science and Technology of China,Hefei 230052,P.R.China)a(Technical Center of Anhui China Tobacco Industry Corporation,Hefei 230088,P.R.China)  
A new 1-naphthalenamine(NNA) specific molecularly imprinted polymer(MIP) was synthesized based on non-covalent interaction.The molecular recognition characteristics of the template polymer were evaluated by UV,IR,XPS and 1H NMR.The NNA-MAA complexes of 1∶1 mole ratio were obtained by nitrogen bonding and the complexes possessed better stabilization(K=5.537×104L/mol).Furthermore,hydrogen atom of the amino group in 1-naphthalenamine is hydrogen-bond acceptors.Hydrogen atom of the lactam group in methacrylic acid is hydrogen-bond donor,being the predominant binding sites interacting with 1-naphthalenamine.The adsorption characteristics of MIP was evaluated by equilibrium adsorption experiment.The results indicate that MIP performs highly selectivity to 1-naphthalenamine.
【Fund】: 安徽中烟工业公司科技创新项目(No.20091009)
【CateGory Index】: O631.3
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