Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Materials for Mechanical Engineering》 2009-04
Add to Favorite Get Latest Update

Preparation of SnO_2 Ultrafine Particles by Spray Pyrolysis Method and Optimization of Technological Parameters

LI Qi-hou,HE Feng,GAO Yu-bo,LIU Zhi-hong,LIU Zhi-yong(Central South University,Changsha 410083,China)  
With SnCl4·5H2O as precusor,SnO2 ultrafine particles were prepared by spray pyrolysis method.Effects of reaction temperature,precursor solution concentration and gas flow rate on the particle size and morphology of SnO2 particles were investigated.The results show that spherical SnO2 particles with an average size of 1.4 μm,uniform size distribution,good crystallinity and few shells and holes could be obtained under the experimental conditions of reaction temperature of 600 ℃,precursor solution concentration of 0.6 mol·L-1 and carrier gas flow rate of 124 L·h-1.
【Fund】: 国家自然科学基金资助项目(50704038);; 高等学校博士学科点专项科研基金资助项目(20060533004);; 教育部科学技术研究重点资助项目(108170)
【CateGory Index】: TB383.3
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 3 Hits
1 ZHANG Yi\|hua, ZHANG Jing\|xin, WANG Xue\|qin, ZHOU Zhuo\|hua ( Open Lab. of Compr. Util. of Carbon. Resour., Dalian Univ. of Technol., Dalian 116012, China );Preparation and characterization of nanosized SnO_2 particles[J];JOURNAL OF DALIAN UNIVERSITY OF TECHNOLOGY;2000-01
2 WEI Zhi-ren,LI Jun,LIU Chao,LIN Lin,ZHENG Yi-bo,GE Shi-yan,ZHANG Hua-wei,DOU Jun-hong(College of Physics Science and Technology,Hebei University,Baoding 071002,China);Hydrothermal Synthesis of Rutile-structured SnO_2 Nanorod Crystals[J];Journal of Synthetic Crystals;2006-01
3 HU Chun-xia 1, L Wei 2, WU You-shi 2(1. Editorial Board of Journal of Shandong University (Science and Technology),Shandong University, Jinan 250061, China;2. School of Materials Science and Engineering, Shandong University, Jinan 250061, China);Synthesis and property study of nanosize tin oxide particles byreverse microemulsions[J];Journal of Shandong University (Engineering Science);2004-06
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 YANG Minge~1, WANG Junbo~ 1,2 , ZHANG Yan~1, DING Bingjun~2(1 Xi’an Institute of Science & Technology, Xi’an 710048; 2 National Laboratory for Materials Strength, Xi’an Jiaotong University, Xi’an 710049);Effect of La-doped on Structure of Nanosized SnO_2 by Chemical Co-precipitation Method[J];Materials Review;2006-S1
2 NIU Xin-shu1,DU Hui2(1.College of Chemistry & Environmental Science,Henan Normal University,Henan Key Laboratory of Environmental Pollution Control,Xinxiang 453007,China;2.Department of Chemical Engineering,Anyang Institute of Technology,Anyang 455000,China);Preparation of SnO_2 nanopowder by sol-gel method and its gas sensitivity properties[J];Electronic Components and Materials;2007-02
3 ZHANG Jun-qing1,FENG De-rong2,JI Xiang3 ,LI Yu-sheng4(1.School Material Engineering of Inner Mongolia University of Science and Technology,Baotou,014010;2.Baotou Tomorrow Technology Co.,Ltd,Baotou 014010 ;3.School of Life Sciences;4.School of Chemistry and Chemical Engineering ,Inner Mongolia University of Science and Technology,Baotou 014010,China );Preparation of Sn~(4+)-TiO_2 and Research of Photocatalytic Degradation of Phenol[J];China Powder Science and Technology;2005-04
4 LI Xiao, GAO Jing, ZHANG Wei-ying (College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, Fujian 350002, China);Structure characterization of microemulsions and polymers prepared by microemulsion polymerization[J];Journal of Fuzhou University(Natural Sciences Edtion);2001-06
5 ZHANG Yi-bing~ 1,2 (1.Department of Chemistry,Shangrao Normal College,Shangrao 334001; 2.National Center for Nanoscience and Nanotechnology,Beijng 100080);Research on the Nano-SnO_2 Prepared by Chemical Precipitation Method Using the Inorganic Salts as Source Materials[J];Bulletin of the Chinese Ceramic Society;2006-04
6 ZHANG Zhong-suo, ZHANG Xing-tang, CHEN Yan-hui, TIAN Bao-li, CHENG Ke, HUANG Ya-bin and DU Zu-liang Key Lab of Special Functional Material of Henan University, Kaifeng 475001, China;Study on the Preparation of Nanometer Oxide SnO_2 Gas-sensitive Material by Sol-gel Method[J];Spectroscopy and Spectral Analysis;2003-01
7 ZHANG Zhong-suo~1, LIU Xiang-yang~2, XING Qian~1, ZHAO Wei~3, LI Yun-cai~2 (1.Physics and Information Photoelectron College, Henan Kity, Henan Kaifeng 475001, China; 3. Technical Director Examination Test Center of Kaifeng, Henan Kaifeng 475001, China);Research on Photoelectric Properties of SnO_2 with Fe_2O_3 Reuniting the Nanometer Oxide Materials[J];Journal of Henan University (Natural Science);2004-03
8 LIAN Jin-jun~1,LI Xian-guo~1,FENG Li-juan~1,MA Yan-li~2 (1. College of Chemistry & Chemical Engineering, Ocean University of China, Shandong Qingdao 266003, China; 2. Dongya Second Middle School of Qiqihaer, Heilongjiang Qiqihaer 161000, China);Nanometer-scale Stannic Oxide from Sol-gel-freeze Drying Process and Its Characterization[J];Huaxue Shijie (Chemical World);2004-04
9 WANG Zhi-qiang1,2,ZHANG Wei-feng1(1.Favulty of Physics and Electronics,Henan University,Kaifeng 475001,China;2.Department of Personnel,Henan University,Kaifeng 475001,China);Researches on Preparation and Development of Nanometer Tin Dioxide Particles[J];Journal of Huzhou Teachers College;2008-01
10 SU Ling-Hao1,ZHANG Xiao-Gang2 (1.Department of Chemistry,Fuyang Normal College,Fuyang 236041,China;2.Institute of Applied Chemistry,Xinjiang University,Urumqi 830046,China);Preparation of Nanosized SnO_2 by Urease-induced Homogeneous Precipitation[J];Journal of Luoyang Institute of Technology;2005-02
China Proceedings of conference Full-text Database 1 Hits
1 ZHANG Jun-qing,FENG De-rong,LI Yu-sheng,JI Xiang (Material Engineering School, UIST Inner Mongolia, Baotou 014010. Baotou Tomorrow Technology Co. , Ltd,Baotou 014010; College of Chemistry and Chemical Engineering; College of Life Sciences, UIST Inner Mongolia, Baotou 014010,China);Preparation of Sn~(4+) - TiO_2 and Research of Photocatalytic Degradation of Phenol[A];[C];2005
【Secondary Citations】
Chinese Journal Full-text Database 8 Hits
1 Lu Fan;Chen Songying;Peng Shaoyi;Wang Xiaoping(State Key Laboratory of Coal conversion,Institute of Coal Chemistry,Chinese Academy of Sciences,Taiyuan,030001,China)(Taiyuan Electronic Plant, Taiyuan,030024,China);Ultrafine SnO_2 as Low Temperature Gas Sensing Material[J];JOURNAL OF FUNCTIONAL MATERIALS;1995-04
2 ZHANG, Jian-Rong GAO, Lian (State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050);Hydrothermal Synthesis and Characterization of SnO_2 Nanoparticles[J];Acta Chimica Sinica;2003-12
3 LUN Ning 1,HU Chun-xia 2,WU You-shi 2* (1.Center of HRTEM Analysis,School of Materials Sci.and Eng.,Shandong Univ.,Jinan 250061,China;2.School of Materials Sci.and Eng.,Shandong Univ.,Jinan 250061,China);Effects of Cu doping on the microstructure, morphology and optic alproperties of nanocrystalline tin oxide[J];Journal of Shandong University of Technology;2003-06
4 ZHANG Jian-Rong, GAO Lian (State Key Lab of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 20050, China);Hydrothermal Synthesis of Tin Oxide Nanoparticles[J];Journal of Inorganic Materials;2004-05
5 ZHU Gui-Sheng, XU Hua-Rui, LIAO Chun-Tu (Guilin University of Electronic Technology, Guilin 541004, China; Liuzhou China-tin Group Company Ltd., Liuzhou 545006, China);Monodispersed Tin Doped Indium Oxide Nanometer Powders Prepared by Hydrothermal Method[J];Journal of Inorganic Materials;2005-02
6 Yan Dongsheng(State Key Laboratory on High Performance Ceramics and Superfine Microstructure Studies,Shanghai Institute of Ceramics, Chinese Academy of Sciences Shanghai 200050 China);Synthesis and Fabrication of Nanostructured Materials[J];JOURNAL OF INORGANIC MATERIALS;1995-01
7 Fang Guojia;Liu Zuli;Hu Yifan;Yao Kailun(Deportment of Physics, Huazhong Univ. of Set.& Tech. Wuhan 430074 China)(International Center for Material Physics, Academica Sinica Shenyang 110015 China)(CCAST(World Laboratory), P.O.Box 8730 Beijing 100080 China;Preparation and Characterization of CuO-SnO_2 Nanocrystalline Powders by the Sol-Gel Method[J];JOURNAL OF INORGANIC MATERIALS;1996-03
8 SHI Juan 1,2 WU Shi-Hua *,1 WANG Shu-Rong 1 ( 1 Department of Chemistry,Nankai University,Tianjin300071);Synthesis of Nanocrystalline SnO_2 via Gel Hydrothermal from Salts of Tin in Different Oxidation States[J];Chinese Journal of Inorganic Chemistry;2004-02
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved