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《Materials for Mechanical Engineering》 2013-01
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Preparation and Properties of CaO-Al_2O_3-SiO_2 Glass-Ceramics Prepared from Waste Materials by Direct Sintering

PENG Chang-hao,LU Jin-shan(School of Materials Science and Engineering,Nanchang Hangkong University,Nanchang 330063,China)  
Taking waste glass,fly ash and calcia as raw materials,CaO-Al2O3-SiO2(CAS) glass-ceramics were prepared from by the direct sintering method,and effects of CaO content and sintering temperature on sintering properties,crystalline composition,microstructure and bending strength of CAS glass-ceramics were studied.The results show that bulk density of the glass-ceramics initially increased and then decreased with the increase of CaO content and sintering temperature,and high CaO adding amount and sintering temperature could promote formating column-shaped wollastonite phase.The bending strength of CAS glass-ceramics exhibited the same tendency as bulk density.The CAS glass-ceramic prepared by 18wt% CaO showed maximum bulk density of 2.26 g·cm-3 after it was sintered at 1 100 ℃ for 2 h,its cystalline phase was a single wollastonite structure with a crystallinity degree of 50.7 % and maximum bending strength of 81.5 MPa.
【Fund】: 江西省研究生创新基金项目(YC10A111)
【CateGory Index】: TQ171.1
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