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《Materials for Mechanical Engineering》 2013-10
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Mesoporous ZrO_2 Nanowire Synthesis by Anodic Alumina Template and Its Photoluminescence Property

L Ren-jiang;ZHANG Fu-xiang;LI Ying-jie;HOU Xue-gong;School of Chemistry and Chemical Engineering,Qiqihar University;  
The precursor was prepared using P123as porogen,ZrOCl as zirconium source and ethanol as solvent,then assembled into nano-channels of anodic aluminum oxide(AAO)templates by vacuuming and pressureinduced technology.After heat treatment,one-dimensional ZrO2 nanomaterials with mesoporous structure were fabricated within the nano-holes of AAO templates.The obtained samples were characterized in detail by SEM, TEM,XRD,EDS and N2 sorption and desorption.The results show that the synthesized ZrO2 nanowires were 60nm in diameter,121.6m2·g-1 in specific surface area,had a homogeneously distributed mesoporous structure with pore diameter of 8nm,and owned good photoluminescence property.
【CateGory Index】: TB383.1
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