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《Acta Optica Sinica》 2008-01
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Growth and Optical Properties of Near-Stoichiometric Ni~(2+)-Doped Lithium Niobate Crystal

Zhang Sichun Xia Haiping Wang Jinhao Zhang Yuepin(Key Laboratory of Photo-Electronic Materials,Ningbo University,Ningbo,Zhejiang 315211,China)  
The near-stoichiometric LiNbO_3(SLN) single crystals doped Ni2+ in 0.5% molar fraction in the raw compositions were grown by the Bridgman method under the conditions of taking K_2O as flux and at a big temperature gradient for solid-liquid interface.The Absorption spectrum of Ni2+ doped crystal was measured.The 381 nm,733 nm and 1280 nm,which are ascribed to spin allowed 3A_2g(F)→3T_1g(P),3A_2g(F)→3T_1g(F),3A_2g(F)→3T_2g(F) transitions of Ni2+ ions in octahedral co-ordination,and 430 nm and 840 nm,which are attributed to spin forbidden 3A_2g(F)→1T_2g(D) and 3A_2g(F)→1E(D) transitions,were observed.The molar fraction ratio of x(Li+)/x(Nb5+) was estimated from the Absorption edge of the crystal to be 0.981.The crystal field strength of Ni2+ doped in SLN crystal,D_q=781 cm-1,the Racah parameter B=1096 cm-1 and C=4353 cm-1 were calculated from the Absorption spectrum and crystal splitting theory.The emission spectra of crystal in the visible region were investigated under various light excitation,and the emission bands at 500~630 nm,800~850 nm were observed and ascribed to the d-d transition 1T_2g(D)→3A_2g(F),1T_2g(D)→3T_2g(F) of Ni2+ in octahedral sites,respectively.
【Fund】: 浙江省科技厅(2007C21121);; 宁波市科技局(2005B100026);; 浙江省教育厅(20061660)资助课题
【CateGory Index】: O782
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