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《Strait Pharmaceutical Journal》 2006-01
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Determination of Ephedrine Hydrochloride in Tianyi Zhike Syrup by HPLC

GAO Min(Putian Institute for Drug Control,Putian 351100,China)  
OBJECTIVE To establish a method for determination of Ephedrine Hydrochloride in Tianyi Zhike Syrup.METHODS Using a HPLC method with Angilent C_(18)(4.6mm×150mm;5μm)column,the mobile phase was methanol-0.025mol·L~(-1) potassium dihydrogen phosphate solution(pH adjusted to 3.0 by phosphoric acid)(12:88),the detection wavelength at 206nm,flow rate was 1.0ml·min~(-1),and the injection volume was 10μL.RESULTS The standard curve of Ephedrine Hydrochloride was rectilinear within the range of 0.1064μg~0.9576μg,r=0.9999.The average recoveries was 100.2%,RSD=0.96%.CONCLUSION The method was accurate 、simple and rapid,it can be used for the method of determination.
【CateGory Index】: R927.2
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Chinese Journal Full-text Database 5 Hits
1 XIE Bai-Mei1,QI Hao-Wen1,ZHAO Rui1,LIN Xiao-Ping2 1Department of Respiratory Medicine, Xijing Hospital, Fourth Military Medical University, Xi'an 710033,China,2Department of Allergy Medicine,Shenyang General Hospital,Shenyang Millitary Area Command,Shenyang 110016,China;Effects of zanthoxylum seed oil on mast cells and tryptase of asthmatic models in guinea pigs[J];Journal of the Fourth Military Medical University;2006-23
2 Wang Fengyi,Jia Yuxin,Li Shengcai,Wang Xiaorong,Liu Fenglin,Chu Huiyuan(Gansu College of TCM,730000,Lanzhou,China);Effects of Zisujian that is ancient formula of Dunhuang on the contents of NO and ET-1 in the serum and lung tissue of rats with chronic bronchitis[J];Journal of Gansu College of Traditional Chinese Medicine;2006-02
3 LIU Hong-xu 1,CHEN Hai-bin 2,WU Chun-min 2(1.Fujian College of Traditional Medicine,Fuzhou 350003;2.Fujian Institute for Drug Control,Fuzhou 350001,China);Advances of Studies on Perilla Frutescens Seeds[J];Strait Pharmaceutical Journal;2004-04
4 LI Jia,DENG Zhi-xu,HUANG Jian-you,LONG Jie-chao(Guangxi Institute of Traditional Medical and Pharmaceutical Sciences,Nanning 530022,China);Identification and quantitative determination of berberine hydrochloride of Niaoyanqing tablet[J];West China Journal of Pharmaceutical Sciences;2007-01
5 Yu Zepu et al Yunnan College of TCM;A Study on the Main Pharmacodynamics of Zhike Pingchuan San[J];Chinese Journal of Ethnomedicine and Ethnopharmacy;1999-06
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