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《Journal of Hebei University(Natural Science Edition)》 2007-01
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Analysis of the Residuals of Trace Quinolones in the Pig Viscera by MEKC Using Sweeping Technique

ZHAO Yan-yan1,2,WANG Li-juan1,LI Zhi-ping3,LI Yue-qiu2,HAN Yuan-yuan2(1.Pharmacy College,Hebei University,Baoding 071002,China;2.Expriment Center of Medical Department,Hebei University,Baoding 071000,China;3.Control Institute of Veterinary Bioproducts and pharmaceuticals of Hebei Province,Shijiazhuang 050051,China)  
Optimum conditions for the determination of trace quinolones,ciprofloxacin ofloxacin and enrofloxacin,in the pig viscera,by micellar electrokinetic chromatography(MEKC) using sweeping as on-line concentration methods were developed.In the running buffer of 20 mmol/LNa2B4O7 +80 mmol/L sodium dodecyl sulfate(SDS)(pH=9.6),ciprofloxacin,ofloxacin and enrofloxacin in the pig viscera were successfully separated and detected within 200 s on a non-coating fused-silica capillary column(48.5 cm×75 μm,effective length 40 cm) at UV detection at 278 nm,separation voltage of 18 kV,the injection pressure of 1.5 kPa,the viscera samples were deproteinized with trichloroacetic acid,and allowed up to 600-fold accumulation concentration of ciprofloxacin.The detection limits of ciprofloxacin,ofloxacin and enrofloxacin was 0.007,0.016 and 0.020 mg/L respectively.The MEKC method based on on-line sweeping technique can be used to separate and detect the residuals of trace medicines in animal food.
【Fund】: 河北省科技攻关资助项目(05276101D-88 42761220);; 河北省中医药管理局资助项目(05015);; 河北大学人才引进资助项目(y2004039);; 河北大学自然科学基金资助项目(2005Y08)
【CateGory Index】: R155
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