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《China Synthetic Fiber Industry》 2006-05
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Dyeing kinetics and thermodynamics study of PA6 fiber modified by compound amine

Guo Xitao,Zhao Yaoming , Ning Ping , Li Linkai (College of Materials Science and Technology , South China University of Technology, Guangzhou 510640;Guangdong Rongtai Industry Co. , Ltd, Jieyang 522000)  
A fixed amount of reactive compound amine ( HAS) modifier was introduced during the hydrolytic polymerization of caprolactam to produce PA6 resin containing HAS which was spun into PA6 fiber. The thermodynamics and kinetics parameters of dyeing HAS modified PA6 fiber with blue acid AGL dye were studied. The results showed that after modification at 90℃, the dye affinity was increased from 22. 01 kJ/mol to 23. 35 kJ/mol, the absolute dyeing enthalpy was decreased from 5. 99 kJ/mol to 2. 16 kJ/mol, the dyeing entropy was increased from 44. 06 J/mol·K to 58. 37 J/mol·K, the dyeing diffusion coefficient was increased from 1. 24×10-14m2/s to 1. 53×10-14m2/s, and the dyeing activation energy was decreased from 14. 89 kJ/mol to 10. 05 kJ/mol. Acid AGL dyes were easier to be dyed on the fiber after modification, which indicated that the dyeing behavior of the modified fiber in acid dyes was improved.
【CateGory Index】: TQ342.11
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