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《Chemical Industry Times》 2012-06
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Study of Synthesis of m-Methoxyphenol

Han Ying1,2 Fu Donglin1 Yao Yong1 Zhou Lina2 Yan Chaoguo1(1 College of Chemistry and Chemical Engineering,Yangzhou University,Jiangsu Yangzhou 225002)(b School of Chemistry and Chemical Engineering,Nanjing University,Jiangsu Nanjing 210093)  
m-Methoxyphenol was prepared in toluene/H2O solution in the presence of phase transfer catalyst by resorcinol and dimethyl sulfate as raw materials.The influence on the rate of production of m-methoxyphenol about different of catalyst,ratio of mole,react temperature and react time was discussed by using orthogonal design.The optimum reaction conditions were specified as follows: TBAB as catalyst,mole ratio of 1∶1.2,the reaction temperature was 80 ℃ and the reaction time was 8 hours.The yield reached 66%.
【Fund】: 国家自然科学基金(No.21172190)项目资助;; 江苏高校优势学科建设工程项目资助
【CateGory Index】: TQ243.12
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【Co-citations】
Chinese Journal Full-text Database 10 Hits
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3 ZHEN Yu-hong,HUANG Shan-shan (Department of Pharmaceutical Chemistry,Dalian Medical University,Dalian 116027,China);Synthesis of analogue of P6A[J];Journal of Dalian Medical University;2003-04
4 CUI Zhi ming, LIU An chang (Department of Technology and Production, Wuhan Institute of Chemical Technology, Wuhan 430074, China);Preparation of Propargyl Chloride[J];Plating and Finishing;2001-02
5 Wei Shumei (Jiangsu Xuzhou Medical Higer Vocational School,Xuzhou 221116);Synthesis of 3-bromobenzaldehyde craft optimization research[J];Chemical Engineering & Equipment;2008-10
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7 WANG Feng- wu (Huainan Teachers′ College,Huainan 232001);Olefin′ s Electropholic Addition Reaction Mechanism and Stereoselectivity[J];Journal of Huaibei Industry Teachers College (Natural Sciences Edition);2001-01
8 LI Dejiang SUN Bihai LI Bin (Department of Chemistry, Yunyang Teachers College, Danjiangkou 442700 ) (Department of Engineering, Wuhan Institute of Chemical Technology, Wuhan 430073);The Application of Beckmann Rearrangement Reaction in Organic Synthesis[J];Journal of Chemical Education;2004-03
9 LI Dejiang~1 SUN Bihai~2 LI Bin~2 (1.Department of Chemistry of Yunyang Normal School,Danjiangkou Hubei Province 442700) (2.Department of Pharmaceutical Engineering of Wuhan Institute of Chemical Engineering 430073);Application of Hofmann Rearrangement Reaction in Organic Synthesis[J];Chemical Education;2006-04
10 Yin Xin(Department of Medicine College,JiangXi Science and Technology Normal University,Nanchang 330013,China);Application of Organosilicon Compounds in Synthesis[J];Guangdong Chemical Industry;2008-10
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