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《Chemical Industry and Engineering Progress》 2009-10
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Preparation of homoharringtonine imprinted polymer by precipitation polymerization

LI Hui1,2,FU Zaide1,SHI Hui1,2,ZHANG Zhaohui2,LI Zhiping2,YANG Zhaoxia2,SHI Aihua2 (1 Hunan Provincial Key Laboratory of Forest and Chemical Engineering,Jishou University,Zhangjiajie 427000,Hunan,China; 2 School of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,Hunan,China)  
The precipitation polymerization method was optimized by using a L9(34) orthogonal factorial design for the preparation of homoharringtonine imprinted polymer (HIP). Optimization of the synthesis condition for the HIP was performed by investigating the influence of four factors,i.e. solvent (acetonitrile) dosage (A),reaction temperature (B),functional monomer (methacrylic acid,MAA) dosage (C) and crosslinker (ethylene glycol dimethyl acrylate,EGDMA) dosage (D),and the interaction of such factors on the adsorption capacity of HIP obtained under different conditions to the template molecule. The results indicated that the influence of these factors on the adsorption capacity of the HIP decreased in the order of C,D,A and B and the optimized synthesis condition was as follows:0.12 mmol MAA,0.4 mmol EGDMA,2.5 mL acetonitrile,reaction temperature at 65 ℃ under the fixed template dosage (0.01 mmol). Also,the interaction of such factors could influence the adsorption capacity of HIP to the template.
【Fund】: 湖南省教育厅青年项目资助课题(06B0706)
【CateGory Index】: O631.3
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