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《Journal of Heilongjiang Bayi Agricultural University》 2017-03
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Simultaneous Determination of Synthetic Colorants by Ionic Liquid Dispersive Liquid-Liquid Microextraction Coupled with High Performance Liquid Chromatography in Carbonated Drink

Sun Peng;Zhu Jianbo;Gao Yuling;Heilongjiang Bayi Agricultural University;Food and Drug Service Center of Market Supervision Administration,Sartu District;  
A novel method for the determination of two synthetic colorants ponceau 4R and sunset yellow from the carbonated drink was developed using ionic liquid dispersive 1iquid-liquid microextraction coupled with high performance liquid chromatography.The influence of extraction parameters including types of extraction solvent,volume of extraction solvent,types of dispersant solven,p H,sodium chloride mass fraction were investigated.Using 160 μL 1-octyl-3-methylimidazolium hexafluorophosphate([OMIM]PF6)as extraction drop,1 000 μL acetonitrile as dispersant solvent,sodium chloride mass fraction 6%,p H was adjusted 4.5 Under the optimal condition,good linear relationship was obtained in the two synthetic colorants concentrations of 1-250 μg·L-1 with the correlation coefficients of 0.998 8-0.999 2;the detection limits were 0.43-1.27 μg·L-1.The proposed method was applied to the determination of two synthetic colorants in carbonated drink,the recoveries were from 88.7% to 98.5%,with the corresponding relative standard deviations were from 1.3% to 5.4%. The method was simple,fast and precise to satisfy,which could meet the requirements for the determination of synthetic colorants in carbonated drink.
【Fund】: 大庆市指导性科技计划项目(szdfy-2015-50);; 黑龙江八一农垦大学(校内培育课题资助计划:XZR2014-17)
【CateGory Index】: O657.72;TS275.3
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【Citations】
Chinese Journal Full-text Database 10 Hits
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【Co-citations】
Chinese Journal Full-text Database 9 Hits
1 Sun Peng;Zhu Jianbo;Gao Yuling;Heilongjiang Bayi Agricultural University;Food and Drug Service Center of Market Supervision Administration,Sartu District;;Simultaneous Determination of Synthetic Colorants by Ionic Liquid Dispersive Liquid-Liquid Microextraction Coupled with High Performance Liquid Chromatography in Carbonated Drink[J];黑龙江八一农垦大学学报;2017-03
2 GAO Yuling;GUO Xiujuan;QIAO Shi;SUN Peng;Heilongjiang Bayi Agricultural University;Heilongjiang Bayi Agricultural University of Mudanjiang Food and Bio Technology Innovation Institute;Weihai Ocean Vocational College;;Ultrasound-assisted Dispersive Liquid-liquid Microextraction Based on the Solidification of a Floating Organic Droplet Followed by Gas Chromatography for the Determination of Five Pyrethroid Pesticides in Tea Samples[J];茶叶科学;2017-03
3 SUN Meng-yuan;SHI Zhi-hong;LI Jian-xun;WU Xing-qiang;HU Xue-yan;ZHANG Bo-lun;FAN Chun-lin;College of Chemistry and Environmental Science,Hebei University;Chinese Academy of Inspection and Quarantine;School of Food and Chemical Engineering,Beijing Technology and Business University;;Determination of 7 Pyrethroid Pesticide Residues in Tea by Gas Chromatography-Triple Quadrupole Mass Spectrometry Combined with Dispersive Solid-phase Extraction and Dispersive Liquid-Liquid Microextraction[J];分析测试学报;2017-05
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6 SUN Peng;GAO Yu-ling;WANG Jin-mei;LIU Xiu-juan;Testing Centre,Heilongjiang Bayi Agricultural University;School of Chemistry and Materials Science,Heilongjiang University;Inspection Center of Daqing Petrochemical Company;;Determination of Eugenol Residue in Aquatic Using Dispersive Liquid-Liquid Microextraction Based on the Solidification of a Floating Organic Droplet Followed by UHPLC-MS/MS[J];质谱学报;2017-03
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【Secondary Citations】
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